Enviar artigo por via de e-mail Synthesis and Features of Crystal Structure of Scandium Hexa(isothiocyanato)chromate(III) Complex with Nicotinic Acid
- Autores: Cherkasova E.V.1, Pervukhina N.V.2, Kuratieva N.V.2,3, Cherkasova T.G.1
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Afiliações:
- Kuzbass State Technical University
- Nikolaev Institute of Inorganic Chemistry, Siberian Branch
- Novosibirsk State University
- Edição: Volume 63, Nº 6 (2018)
- Páginas: 776-780
- Seção: Coordination Compounds
- URL: https://journal-vniispk.ru/0036-0236/article/view/168758
- DOI: https://doi.org/10.1134/S0036023618060050
- ID: 168758
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Resumo
A double complex compound with a polymeric cation of composition [Sc2(C6H5NO2)3(C6H4NO2)3][Cr(NCS)6] has been synthesized by the reaction between Sc(NO3)3, K3[Cr(NCS)6], and nicotinic acid (C5H5NCOO) in an aqueous solution and studied by chemical analysis, IR spectroscopy, and X-ray diffraction. Crystals are hexagonal, space group P6322, Z = 2; a = 12.995(2) Å, c = 17.864(3) Å, V = 2612.3(7) Å3, ρcalc = 1.559 g/cm3.
Sobre autores
E. Cherkasova
Kuzbass State Technical University
Autor responsável pela correspondência
Email: ctg.htnv@kuzstu.ru
Rússia, Kemerovo, 650000
N. Pervukhina
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: ctg.htnv@kuzstu.ru
Rússia, Novosibirsk, 630090
N. Kuratieva
Nikolaev Institute of Inorganic Chemistry, Siberian Branch; Novosibirsk State University
Email: ctg.htnv@kuzstu.ru
Rússia, Novosibirsk, 630090; Novosibirsk, 630090
T. Cherkasova
Kuzbass State Technical University
Email: ctg.htnv@kuzstu.ru
Rússia, Kemerovo, 650000
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