Synthesis, Crystal Structure, and Biological Activity of 1,3,5-Thimethyl-2,4,6-tris(3'-methyl-1'-imidazoliomethylene)Benzene Perchlorate

J.-F. Lu; C.-B. Zhao; J. Shi; L.-X. Jin; G.-X. Hua; H.-G. Ge

doi:10.1134/S1063774517070185

Synthesis, Crystal Structure, and Biological Activity of 1,3,5-Thimethyl-2,4,6-tris(3'-methyl-1'-imidazoliomethylene)Benzene Perchlorate

Autores: Lu J.¹, Zhao C.¹, Shi J.¹, Jin L.¹, Hua G.¹, Ge H.¹
Afiliações:
1. College of Chemical and Environment Science, The Institute of Catalysis Science and Technology
Edição: Volume 62, Nº 7 (2017)
Páginas: 1051-1054
Seção: Structure of Organic Compounds
URL: https://journal-vniispk.ru/1063-7745/article/view/191633
DOI: https://doi.org/10.1134/S1063774517070185
ID: 191633

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Resumo

The title compound, C₂₄H₃₃C_l3N₆O₁₂(ClO₄)₃, was synthesized and structurally characterized by elemental analysis, IR, MS, HMR and single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P1, Z = 2. The crystal structure is stabilized by C–H···O hydrogen-bonds forming a three-dimensional network. The preliminary biological test showed that the title compound had anti-Mycobacterium phlei 1180 activity.