Analysis of the Structural Evolution of Zinc Oxide Powders Obtained by Mechanical High-Energy Grinding


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Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallites, increase in specific surface area, as well as changes in the number and ratio of adsorption centers, has been demonstrated. The data on the reconstruction of the surface of zinc oxide powders and multiple bond breaking in near-surface areas resulting from long-term dispersion have been presented.

作者简介

I. Averin

Penza State University

Email: pronin_i90@mail.ru
俄罗斯联邦, Penza, 440026

I. Pronin

Penza State University; St. Petersburg State Electrotechnical University LETI

编辑信件的主要联系方式.
Email: pronin_i90@mail.ru
俄罗斯联邦, Penza, 440026; St. Petersburg, 197022

N. Yakushova

Penza State University

Email: pronin_i90@mail.ru
俄罗斯联邦, Penza, 440026

A. Karmanov

Penza State University

Email: pronin_i90@mail.ru
俄罗斯联邦, Penza, 440026

M. Sychev

St. Petersburg State Technological Institute (Technical University); Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences

Email: pronin_i90@mail.ru
俄罗斯联邦, St. Petersburg, 190013; St. Petersburg, 199034

S. Vikhman

St. Petersburg State Technological Institute (Technical University)

Email: pronin_i90@mail.ru
俄罗斯联邦, St. Petersburg, 190013

V. Levitsky

Research and Development Center for Thin-Film Technologies in Energetics

Email: pronin_i90@mail.ru
俄罗斯联邦, St. Petersburg, 194064

V. Moshnikov

Penza State University; St. Petersburg State Electrotechnical University LETI

Email: pronin_i90@mail.ru
俄罗斯联邦, Penza, 440026; St. Petersburg, 197022

E. Terukov

Ioffe Institute, Russian Academy of Sciences

Email: pronin_i90@mail.ru
俄罗斯联邦, St. Petersburg, 194022

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