Microwave synthesis of new azolyl-substituted thiazolo[5,4- d ]thiazoles

L. K. Papernaya; A. A. Shatrova; A. V. Kletskov; S. K. Petkevich; I. V. Sterkhova; L. V. Klyba; G. G. Levkovskaya

doi:10.1134/S107042801704008X

Microwave synthesis of new azolyl-substituted thiazolo[5,4-d]thiazoles

作者: Papernaya L.K.¹, Shatrova A.A.¹, Kletskov A.V.², Petkevich S.K.², Sterkhova I.V.¹, Klyba L.V.¹, Levkovskaya G.G.¹
隶属关系:
1. Favorskii Irkutsk Institute of Chemistry, Siberian Branch
2. Institute of Physical Organic Chemistry
期: 卷 53, 编号 4 (2017)
页面: 550-556
栏目: Review
URL: https://journal-vniispk.ru/1070-4280/article/view/216056
DOI: https://doi.org/10.1134/S107042801704008X
ID: 216056

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One-pot condensation of dithiooxamide with 4,5-dichloro-1,2-thiazole-3-carbaldehyde and 5-phenyl-1,2-oxazole-3-carbaldehyde, followed by oxidation of intermediate 2,5-dihydro[1,3]thiazolo[5,4-d]-[1,3]thiazoles with selenium dioxide, afforded previously unknown 2,5-bis(4,5-dichloro-1,2-thiazol-3-yl)- and 2,5-bis(5-phenyl-1,2-oxazol-3-yl)[1,3]thiazolo[5,4-d][1,3]thiazoles as first representative of bis-isothiazolyl- and bis-isoxazolyl thiazolothiazoles.