Synthesis of ethyl ({[adamantan-1(2)-ylalkyl]-carbamothioyl}amino)acetates


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详细

Reactions of adamantan-1(2)-amines and adamantan-1(2)-ylalkanamines with ethyl isothiocyanatoacetate afforded ethyl ({[adamantan-1(2)-ylalkyl]carbamothioyl}amino)acetates in 85–95% yields. The hydrolysis of ethyl {[(adamantan-2-yl)carbamothioyl]amino}acetate in alkaline medium resulted in the formation of {[(adamantan-2-yl)carbamothioyl]amino}acetic acid in a virtually quantitative yield.

作者简介

V. Burmistrov

Volzhskii Polytechnic Institute (Branch) at Volgograd State Technical University

Email: butov@volpi.ru
俄罗斯联邦, ul. Engelsa 42a, Volzhskii, 404131

D. Pitushkin

Volzhskii Polytechnic Institute (Branch) at Volgograd State Technical University

Email: butov@volpi.ru
俄罗斯联邦, ul. Engelsa 42a, Volzhskii, 404131

V. Vasipov

Peter the Great St. Petersburg Polytechnic University

Email: butov@volpi.ru
俄罗斯联邦, St. Petersburg

G. Butov

Volzhskii Polytechnic Institute (Branch) at Volgograd State Technical University

编辑信件的主要联系方式.
Email: butov@volpi.ru
俄罗斯联邦, ul. Engelsa 42a, Volzhskii, 404131

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