Influence of Lithium on the Structure and Phase Composition Formation in the Synthesis of Hydroxyapatite


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The influence of lithium substitution for calcium over a broad concentration range (0–20 mol %) on the crystal lattice parameters, coherent scattering regions, and phase composition was studied for hydroxyapatite synthesized by precipitation from solutions and heat treatment at 900, 1200, and 1400°C. The lithium substitution in a more than 10 mol % concentration and increase in the heat treatment temperature to 1400°C give rise to a complex phase composition, which includes not only the apatite phase, but also two tricalcium phosphate phases and calcium pyrophosphate. The results are useful for the development of hydroxyapatite-based materials for bone surgery.

作者简介

V. Smirnov

Baikov Institute of Metallurgy and Materials Science

编辑信件的主要联系方式.
Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

S. Smirnov

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

A. Krylov

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

O. Antonova

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

M. Goldberg

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

T. Obolkina

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

A. Konovalov

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

A. Leonov

Moscow State University

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119899

S. Barinov

Baikov Institute of Metallurgy and Materials Science

Email: smirnov2007@mail.ru
俄罗斯联邦, Moscow, 119991

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