Email this article Synthesis and crystal structure of (2-chloro-4-(phenylthio)phenyl) (3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone
- Authors: Sun G.1, Zhai Z.2, Sun Z.2, Tan C.2, Weng J.2, Liu X.2
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Affiliations:
- School of Chemistry and Chemical Engineering
- College of Chemical Engineering
- Issue: Vol 58, No 8 (2017)
- Pages: 1663-1667
- Section: Article
- URL: https://journal-vniispk.ru/0022-4766/article/view/161721
- DOI: https://doi.org/10.1134/S002247661708025X
- ID: 161721
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Abstract
(2-Chloro-4-(phenylthio)phenyl)(3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone was obtained by accident. In order to know the structure of this product, the compound was isolated by column chromatography and recrystallized from EtOH. The compound was characterized by X-ray diffraction. The compound crystallized in the triclinic space group P-1 with a = 9.909(2) Å, b = 11.824(2) Å, c = 13.056(3) Å, α = 63.309(3)°, β = 89.964(4)°, γ = 67.727(3)°, V = 1237.7(4) Å3, Z = 2 and R = 0.0414.
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About the authors
G.-X. Sun
School of Chemistry and Chemical Engineering
Email: xhliu@zjut.edu.cn
China, Jiangsu, Yancheng
Z.-W. Zhai
College of Chemical Engineering
Email: xhliu@zjut.edu.cn
China, Hangzhou, Zhejiang
Z.-H. Sun
College of Chemical Engineering
Email: xhliu@zjut.edu.cn
China, Hangzhou, Zhejiang
C.-X. Tan
College of Chemical Engineering
Email: xhliu@zjut.edu.cn
China, Hangzhou, Zhejiang
J.-Q. Weng
College of Chemical Engineering
Email: xhliu@zjut.edu.cn
China, Hangzhou, Zhejiang
X.-H. Liu
College of Chemical Engineering
Author for correspondence.
Email: xhliu@zjut.edu.cn
China, Hangzhou, Zhejiang
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