Email this article The Atomic Structure of Cu(II) Acetate-Bipyridine Under Thermal Decomposition: An X-Ray Spectroscopy Study
- Authors: Kremennaya M.A.1, Budnyk A.P.1, Soldatov M.A.1, Lastovina T.A.1, Soldatov A.V.1
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Affiliations:
- The Smart Materials Research Center
- Issue: Vol 59, No 1 (2018)
- Pages: 64-70
- Section: Article
- URL: https://journal-vniispk.ru/0022-4766/article/view/161836
- DOI: https://doi.org/10.1134/S0022476618010109
- ID: 161836
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Abstract
A number of experimental techniques were used to study the changes in the atomic structure of copper(II) acetate-bipyridine under thermal decomposition between 25°C and 700°C to form copper-containing nanoparticles. The dynamics of structural changes during decomposition in a thermogravimetric chamber is compared with X-ray absorption spectra, IR spectra, and diffraction patterns for a sequence of annealing temperatures. The experimental results were used to construct theoretical structural models of the complex under thermal decomposition.
About the authors
M. A. Kremennaya
The Smart Materials Research Center
Author for correspondence.
Email: kremennayamariya@gmail.com
Russian Federation, Rostov-on-Don
A. P. Budnyk
The Smart Materials Research Center
Email: kremennayamariya@gmail.com
Russian Federation, Rostov-on-Don
M. A. Soldatov
The Smart Materials Research Center
Email: kremennayamariya@gmail.com
Russian Federation, Rostov-on-Don
T. A. Lastovina
The Smart Materials Research Center
Email: kremennayamariya@gmail.com
Russian Federation, Rostov-on-Don
A. V. Soldatov
The Smart Materials Research Center
Email: kremennayamariya@gmail.com
Russian Federation, Rostov-on-Don
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