Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3 H -1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

A. V. Pulya; I. I. Seifullina; L. S. Skorokhod; V. I. Pavlovskii; V. Kh. Kravtsov; S. L. Bogza; S. Yu. Suikov

doi:10.1134/S002247661802035X

Molecular and Crystal Structure of the Condensation Product of 2-(7-Bromo-2-Oxo-5-Phenyl-3H-1,4-Benzdiazepin-1-Yl)Acetohydrazide (Gidazepam) with Salicylic Aldehyde

Authors: Pulya A.V.¹, Seifullina I.I.¹, Skorokhod L.S.¹, Pavlovskii V.I.², Kravtsov V.K.³, Bogza S.L.⁴, Suikov S.Y.⁴
Affiliations:
1. Mechnikov Odessa National University
2. Bogatskii Physicochemical Institute
3. Institute of Applied Physics
4. Litvinenko Institute of Physical-Organic Chemistry and Coal Chemistry
Issue: Vol 59, No 2 (2018)
Pages: 497-501
Section: Article
URL: https://journal-vniispk.ru/0022-4766/article/view/161900
DOI: https://doi.org/10.1134/S002247661802035X
ID: 161900

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Abstract

Hydrazone [HydrHSal]∙Н₂О is synthesized for the first time by the interaction of 2-(7-bromo-2-oxo-5- phenyl-3H-1,4-benzdiazepin-1-yl)acetohydrazide (gidazepam) with salicylic aldehyde and characterized by the elemental analysis, thermogravimetry, mass, electron, IR, and NMR spectroscopic techniques. The molecular and crystal structure is determined by single crystal X-ray diffraction.