Synthesis of ceramics based on zirconium and hafnium borides by spark plasma sintering and study of its thermal oxidative stability


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Abstract

Ultra-high-temperature ceramic materials based on zirconium and hafnium borides were obtained by spark plasma sintering. The samples were thermal-shock tested on a gas-dynamic setup in an oxidizing atmosphere; the temperature on the surface of the samples was 2100°C. The microstructure of the samples after sintering and gas-dynamic tests was studied by electron microscopy, X-ray tomography, and elemental analysis.

About the authors

E. N. Pryamilova

JSC Ural Research Institute of Composite Materials; Perm National Research Polytechnic University

Author for correspondence.
Email: pryamilova.en@gmail.com
Russian Federation, ul. Novozvyaginskaya 57, Perm, 614014; Komsomol’skii pr. 29, Perm, 614990

A. A. Efimov

Perm National Research Polytechnic University

Email: pryamilova.en@gmail.com
Russian Federation, Komsomol’skii pr. 29, Perm, 614990

V. I. Mali

Lavrent’ev Institute of Hydrodynamics

Email: pryamilova.en@gmail.com
Russian Federation, Siberian Branch, pr. Lavrent’eva 15, Novosibirsk, 630090

A. G. Anisimov

Lavrent’ev Institute of Hydrodynamics

Email: pryamilova.en@gmail.com
Russian Federation, Siberian Branch, pr. Lavrent’eva 15, Novosibirsk, 630090

Yu. B. Lyamin

JSC Ural Research Institute of Composite Materials

Email: pryamilova.en@gmail.com
Russian Federation, ul. Novozvyaginskaya 57, Perm, 614014

V. Z. Poilov

Perm National Research Polytechnic University

Email: pryamilova.en@gmail.com
Russian Federation, Komsomol’skii pr. 29, Perm, 614990

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