Synthesis of nanocrystalline BiSbO 4

A. V. Egorysheva; A. A. Berseneva; T. B. Kuvshinova; O. M. Gaitko

doi:10.1134/S0036023617090042

Synthesis of nanocrystalline BiSbO₄

Autores: Egorysheva A.V.¹, Berseneva A.A.¹, Kuvshinova T.B.¹, Gaitko O.M.¹
Afiliações:
1. Kurnakov Institute of General and Inorganic Chemistry
Edição: Volume 62, Nº 9 (2017)
Páginas: 1155-1161
Seção: Synthesis and Properties of Inorganic Compounds
URL: https://journal-vniispk.ru/0036-0236/article/view/167984
DOI: https://doi.org/10.1134/S0036023617090042
ID: 167984

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Reaction of hydrochloric acid solutions of bismuth and antimony with ammonia has been studied and effect of coprecipitation conditions of resultant hydroxides on their reactivity has been determined. Annealing conditions for coprecipitation products have been optimized. Effect of surfactants of different nature and concentration on the phase composition, size, and shape of resulting particles have been examined. Nanocrystalline samples of BiSbO₄ have been synthesized.