Synthesis of Silver Nanoclusters and Nanoparticles in the Medium of Hyperbranched Polyester Polyamine, and the Morphology and Aggregation Properties of the Metal–Polymer Nanocomposite

V. A. Prytkov; Прытков В. А.; A. A. Khannanov; Ханнанов А. А.; V. G. Evtyugin; Евтюгин В. Г.; A. R. Gataulina; Гатаулина А. Р.; M. P. Kutyreva; Кутырева М. П.

doi:10.31857/S0044457X22601857

Synthesis of Silver Nanoclusters and Nanoparticles in the Medium of Hyperbranched Polyester Polyamine, and the Morphology and Aggregation Properties of the Metal–Polymer Nanocomposite

Authors: Prytkov V.A.¹, Khannanov A.A.¹, Evtyugin V.G.¹, Gataulina A.R.¹, Kutyreva M.P.¹
Affiliations:
1. Alexander Butlerov Institute of Chemistry, Kazan (Volga Region) Federal University
Issue: Vol 68, No 5 (2023)
Pages: 672-681
Section: НЕОРГАНИЧЕСКИЕ МАТЕРИАЛЫ И НАНОМАТЕРИАЛЫ
URL: https://journal-vniispk.ru/0044-457X/article/view/136370
DOI: https://doi.org/10.31857/S0044457X22601857
EDN: https://elibrary.ru/SMKOPD
ID: 136370

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Abstract
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Abstract

A procedure was developed for the single-step synthesis of a metal–polymer nanocomposite based on silver nanoparticles and second-pseudogeneration superbranched polyester functionalized along the periphery with 3-[(2-aminoethyl)amino]propionate. Under the conditions of the synthesis in the medium of H2O or DMSO, hyperbranched polyester decorated with ethylenediamine moieties can act as both a reductant of the nanoscale silver state and a stabilizer of it. The synthesized composite nanomaterial is formed by aggregates of hyperbranched polyester polyamine doped with Ag(0) nanoclusters and nanoparticles of spheroidal symmetry with a face-centered cubic crystal lattice. The hydrodynamic diameter of aggregates and the diameter of particles increase with increasing molar ratio
and are 34–90 and 7–14 nm, respectively.

Keywords

silver nanoparticles, hyperbranched polymers, composite materials

References

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