Heteroleptic Metal-Organic Frameworks of Lanthanides (Lа, Ce, and Ho) Based on Ligands of the Anilate Type and Dicarboxylic Acids

O. Yu. Trofimova; Трофимова О. Ю.; A. V. Maleeva; Малеева А. В.; K. V. Arsen’eva; Арсеньева К. В.; A. V.  Klimashevskaya; Климашевская А. В.; A. V. Cherkasov; Черкасов А. В.; A. V. Piskunov; Пискунов А. В.

doi:10.31857/S0132344X22600473

Heteroleptic Metal-Organic Frameworks of Lanthanides (Lа, Ce, and Ho) Based on Ligands of the Anilate Type and Dicarboxylic Acids

作者: Trofimova O.Y.¹, Maleeva A.V.¹, Arsen’eva K.V.¹, Klimashevskaya A.V.¹, Cherkasov A.V.¹, Piskunov A.V.¹
隶属关系:
1. Razuvaev Institute of Organometallic Chemistry, Russian Academy of Sciences, Nizhny Novgorod, Russia
期: 卷 49, 编号 5 (2023)
页面: 278-289
栏目: Articles
URL: https://journal-vniispk.ru/0132-344X/article/view/137291
DOI: https://doi.org/10.31857/S0132344X22600473
EDN: https://elibrary.ru/POTLZC
ID: 137291

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详细

New heteroleptic metal-organic frameworks of lanthanides, units of which contain anionic organic ligands of two types, are prepared by the solvothermal synthesis in N,N-dimethylformamide (DMF). The cross-linked coordination polymer [Ho2(CA)2(Bdc)·4DMF] (I) and two scaffold derivatives [La2(pQ)2(Bpdc)·4DMF] (II) and [Ce2(CA)(Bdc)2·4DMF]·2DMF (III·2DMF), where CA is chloranilic acid dianion, pQ is 2,5-dihydroxy-3,6-di-tert-butyl-para-benzoquinone dianion, Bdc is terephthalic acid dianion, and Bpdc is 4,4'-biphenyldicarboxylic acid dianion, are synthesized. The structures of compounds I, II, and III·2DMF are studied by X-ray diffraction (XRD) (CIF file CCDC nos. 2212230, 2212231, and 2212232, respectively).

关键词

anilate ligand, metal-organic frameworks, dicarboxylic acids, redox-active ligand, XRD, solvothermal synthesis

参考

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