Compact Aluminum Oxynitride Based Ceramic Obtained by the SHS-Metallurgy Method


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Abstract

SHS-Metallurgy methods were used to obtain samples in the form of aluminum oxynitride Al5O6N ingots (AlON) using mixtures of the thermit type. The experiments were performed in SHS reactors at initial nitrogen pressure 5 MPa. The optimal conditions for the synthesis of the most stable phase of aluminum oxynitride Al5O6N were determined. Regimes were developed for comminuting the synthesized ingots into powder with definite fractions. Spark plasma sintering (SPS) was used to obtain from them experimental samples with high density, hardness, and transparency.

About the authors

V. A. Gorshkov

Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences

Author for correspondence.
Email: gorsh@ism.ac.ru
Russian Federation, Chernogolovka

E. G. Grigor’ev

National Nuclear Research University MIPhI

Email: gorsh@ism.ac.ru
Russian Federation, Moscow

P. A. Miloserdov

Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences

Email: gorsh@ism.ac.ru
Russian Federation, Chernogolovka

V. I. Yukhvid

Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences

Email: gorsh@ism.ac.ru
Russian Federation, Chernogolovka

N. V. Sachkova

Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences

Email: gorsh@ism.ac.ru
Russian Federation, Chernogolovka

N. A. Rubinkovskii

National Nuclear Research University MIPhI

Email: gorsh@ism.ac.ru
Russian Federation, Moscow

A. G. Zholnin

National Nuclear Research University MIPhI

Email: gorsh@ism.ac.ru
Russian Federation, Moscow

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