Morphology and Structure of a Fine-Grained Composite Material Based on Boehmite Extracted from Aqueous Solutions of Na-Carboxymethyl Cellulose with Aluminum Powder


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Abstract

Fine-grained composite material is synthesized from aluminum powder in aqueous solutions of Na-sodium carboxymethyl cellulose. The phase composition of the composite material is determined using X-ray phase analysis and infrared spectroscopy. Aluminum oxyhydroxide (boehmite) stabilized by the polymer material Na-sodium carboxymethyl cellulose is found to be formed during synthesis. The interaction between boehmite and the polymer material is implemented due to intermolecular hydrogen bonds. The formation of 600-nm spherical particles with porous surfaces is revealed by scanning electron microscopy. Unlike traditional methods of producing boehmite at 200–400°С, synthesis occurs at 70–80°С. The prospects of using boehmite for the creation of porous functional materials are shown.

About the authors

N. M. Antonova

Kamensky Institute

Author for correspondence.
Email: melnik1@rambler.ru
Russian Federation, Kamensk-Shakhtinsky, Rostov oblast, 346800

F. M. Boldyrev

Kamensky Institute

Email: melnik1@rambler.ru
Russian Federation, Kamensk-Shakhtinsky, Rostov oblast, 346800

I. Y. Zabiyaka

Don State Technical University

Email: melnik1@rambler.ru
Russian Federation, Rostov-on-Don, 344000

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