Morphology and Structure of a Fine-Grained Composite Material Based on Boehmite Extracted from Aqueous Solutions of Na-Carboxymethyl Cellulose with Aluminum Powder
- Authors: Antonova N.M.1, Boldyrev F.M.1, Zabiyaka I.Y.2
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Affiliations:
- Kamensky Institute
- Don State Technical University
- Issue: Vol 12, No 5 (2018)
- Pages: 974-981
- Section: Article
- URL: https://journal-vniispk.ru/1027-4510/article/view/196026
- DOI: https://doi.org/10.1134/S102745101805021X
- ID: 196026
Cite item
Abstract
Fine-grained composite material is synthesized from aluminum powder in aqueous solutions of Na-sodium carboxymethyl cellulose. The phase composition of the composite material is determined using X-ray phase analysis and infrared spectroscopy. Aluminum oxyhydroxide (boehmite) stabilized by the polymer material Na-sodium carboxymethyl cellulose is found to be formed during synthesis. The interaction between boehmite and the polymer material is implemented due to intermolecular hydrogen bonds. The formation of 600-nm spherical particles with porous surfaces is revealed by scanning electron microscopy. Unlike traditional methods of producing boehmite at 200–400°С, synthesis occurs at 70–80°С. The prospects of using boehmite for the creation of porous functional materials are shown.
About the authors
N. M. Antonova
Kamensky Institute
Author for correspondence.
Email: melnik1@rambler.ru
Russian Federation, Kamensk-Shakhtinsky, Rostov oblast, 346800
F. M. Boldyrev
Kamensky Institute
Email: melnik1@rambler.ru
Russian Federation, Kamensk-Shakhtinsky, Rostov oblast, 346800
I. Y. Zabiyaka
Don State Technical University
Email: melnik1@rambler.ru
Russian Federation, Rostov-on-Don, 344000
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