Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl]benzamide : N,N-dimethylformamide (1 : 1)
- Authors: Sharma P.1, Subbulakshmi K.N.2, Narayana B.2, Sarojini B.K.3, Kant R.1
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Affiliations:
- X-ray Crystallography Laboratory, Department of Physics
- Department of Chemistry
- Industrial Chemistry Division, Department of Studies in Chemistry
- Issue: Vol 61, No 2 (2016)
- Pages: 230-233
- Section: Structure of Organic Compounds
- URL: https://journal-vniispk.ru/1063-7745/article/view/189843
- DOI: https://doi.org/10.1134/S106377451602022X
- ID: 189843
Cite item
Abstract
The title compound, 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl] benzamide:N,N-dimethylformamide (1: 1), (C15H11N3O2S2 · C3H7NO), was synthesized, and its structure was established by spectral analysis and X-ray diffraction studies. The compound crystallizes in the monoclinic space group P21/n with a = 10.8714(7), b = 9.0497(5), c = 19.8347(13) Å, β = 91.093(5)°, Z = 4. The crystal structure is stabilized by N–H···S, C–H···O and N–H···O hydrogen bonds. The π···π interactions are also observed between the rings.
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About the authors
P. Sharma
X-ray Crystallography Laboratory, Department of Physics
Email: rkant.ju@gmail.com
India, Tawi
K. N. Subbulakshmi
Department of Chemistry
Email: rkant.ju@gmail.com
India, Mangalagangotri, D.K.
B. Narayana
Department of Chemistry
Email: rkant.ju@gmail.com
India, Mangalagangotri, D.K.
B. K. Sarojini
Industrial Chemistry Division, Department of Studies in Chemistry
Email: rkant.ju@gmail.com
India, Mangalagangothri, D.K.
R. Kant
X-ray Crystallography Laboratory, Department of Physics
Author for correspondence.
Email: rkant.ju@gmail.com
India, Tawi
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