Structure and mechanical properties of foils made of nanocrystalline beryllium


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Аннотация

The phase composition and structural features of (45–90)-μm-thick foils obtained from nanocrystalline beryllium during multistep thermomechanical treatment have been established using electron microscopy, electron diffraction, electron backscattering diffraction, and energy-dispersive analysis. This treatment is shown to lead to the formation of a structure with micrometer- and submicrometer-sized grains. The minimum average size of beryllium grains is 352 nm. The inclusions of beryllium oxide (ВеО) of different modifications with tetragonal (sp. gr. P42/mnm) and hexagonal (sp. gr. P63/mmc) lattices are partly ground during deformation to a size smaller than 100 nm and are located along beryllium grain boundaries in their volume, significantly hindering migration during treatment. The revealed structural features of foils with submicrometer-sized crystallites provide the thermal stability of their structural state. Beryllium with this structure is a promising material for X-ray instrument engineering and for the production of ultrathin (less than 10 μm) vacuum-dense foils with very high physicomechanical characteristics.

Об авторах

O. Zhigalina

Shubnikov Institute of Crystallography; Bauman Moscow State Technical University

Автор, ответственный за переписку.
Email: zhigal@ns.crys.ras.ru
Россия, Leninskii pr. 59, Moscow, 119333; Vtoraya Baumanskaya ul. 5, Moscow, 105005

A. Semenov

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

A. Zabrodin

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

D. Khmelenin

Shubnikov Institute of Crystallography

Email: zhigal@ns.crys.ras.ru
Россия, Leninskii pr. 59, Moscow, 119333

D. Brylev

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

A. Lizunov

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

A. Nebera

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

I. Morozov

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

A. Anikin

Bochvar High-Technology Scientific Research Institute for Inorganic Materials

Email: zhigal@ns.crys.ras.ru
Россия, ul. Rogova 5, Moscow, 123060

A. Orekhov

Shubnikov Institute of Crystallography

Email: zhigal@ns.crys.ras.ru
Россия, Leninskii pr. 59, Moscow, 119333

A. Kuskova

Shubnikov Institute of Crystallography

Email: zhigal@ns.crys.ras.ru
Россия, Leninskii pr. 59, Moscow, 119333

V. Mishin

Peter the Great St. Petersburg Polytechnic University

Email: zhigal@ns.crys.ras.ru
Россия, Polytechnicheskaya 29, St. Petersburg, 195251

A. Seryogin

Shubnikov Institute of Crystallography; Bauman Moscow State Technical University

Email: zhigal@ns.crys.ras.ru
Россия, Leninskii pr. 59, Moscow, 119333; Vtoraya Baumanskaya ul. 5, Moscow, 105005

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