Low-Voltage Scanning Electron Microscopy and Energy-Dispersive X-Ray Microanalysis of the Interface of Multilayer Polymer Composite
- Authors: Orekhov A.S.1,2, Arkharova N.A.1, Kononova S.V.3, Klechkovskaya V.V.1
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Affiliations:
- Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
- National Research Centre “Kurchatov Institute”
- Institute of Macromolecular Compounds
- Issue: Vol 63, No 5 (2018)
- Pages: 745-748
- Section: Structure of Organic Compounds
- URL: https://journal-vniispk.ru/1063-7745/article/view/192907
- DOI: https://doi.org/10.1134/S1063774518050206
- ID: 192907
Cite item
Abstract
The morphology of the layer of polyelectrolyte complex, which is formed in the composite based on chitosan and sulfoethyl cellulose during the contact of a solution of one of them with a gel film of the other one, has been investigated by the low-voltage (≤3 kV) scanning electron microscopy. A technique for eliminating the effects related to charge accumulation on the dielectric film surface is proposed.
About the authors
A. S. Orekhov
Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”; National Research Centre “Kurchatov Institute”
Email: klechvv@crys.ras.ru
Russian Federation, Moscow, 119333; Moscow, 123182
N. A. Arkharova
Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Email: klechvv@crys.ras.ru
Russian Federation, Moscow, 119333
S. V. Kononova
Institute of Macromolecular Compounds
Email: klechvv@crys.ras.ru
Russian Federation, St. Petersburg, 199004
V. V. Klechkovskaya
Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Author for correspondence.
Email: klechvv@crys.ras.ru
Russian Federation, Moscow, 119333
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