Experimental and Theoretical Study of the Triple-Crystal High-Resolution X-Ray Diffraction Scheme in Reciprocal Space Mapping Technique


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Abstract

The triple-crystal high-resolution X-ray diffraction scheme has been experimentally and theoretically investigated using reciprocal space mapping. The procedure for calculating the spectral angular instrumental functions of diffractometer to take into account the influence of mirror, monochromator, analyzer, and slits on the intensity distribution near reciprocal lattice point is described. Good coincidence of calculated and experimental cross sections of reciprocal space maps (RSMs) is shown by an example of a perfect Si(110) single crystal.

About the authors

A. Yu. Seregin

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences; National Research Centre “Kurchatov Institute”

Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333; Moscow, 123098

P. A. Prosekov

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences; National Research Centre “Kurchatov Institute”

Author for correspondence.
Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333; Moscow, 123098

F. N. Chukhovsky

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences

Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333

Yu. A. Volkovsky

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences; National Research Centre “Kurchatov Institute”

Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333; Moscow, 123098

A. E. Blagov

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences; National Research Centre “Kurchatov Institute”

Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333; Moscow, 123098

M. V. Kovalchuk

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”
Russian Academy of Sciences; National Research Centre “Kurchatov Institute”; St. Petersburg State University

Email: p.prosekov@gmail.com
Russian Federation, Moscow, 119333; Moscow, 123098; St. Petersburg, 199034

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