Email this article Synthesis and characterization of tetraphenylphosphonium salts of N-phosphorylated thioureas and bis-thioureas
- Authors: Samakbaeva M.A.1, Babashkina M.G.2, Isaev A.Y.3, Safin D.A.2,3
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Affiliations:
- Tomsk Polytechnic University
- Institute of Condensed Matter and Nanosciences, Université Catholique de Louvain
- University of Tyumen
- Issue: Vol 67, No 9 (2018)
- Pages: 1738-1741
- Section: Brief Communications
- URL: https://journal-vniispk.ru/1066-5285/article/view/243050
- DOI: https://doi.org/10.1007/s11172-018-2284-3
- ID: 243050
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Abstract
Tetraphenylphosphonium salts of N-phosphorylated thioureas and bio-thioureas were synthesized by the reactions of their sodium salts with PPh4Br in 96% aqueous EtOH. The structures of compounds obtained were studied by IR spectroscopy, 1H and 31P{1H} NMR spectroscopy, and electrospray ionization mass spectrometry; their compositions were confirmed by elemental analysis.
About the authors
M. A. Samakbaeva
Tomsk Polytechnic University
Author for correspondence.
Email: madina.samakbaeva@yandex.ru
Russian Federation, 30 prosp. Lenina, Tomsk, 634050
M. G. Babashkina
Institute of Condensed Matter and Nanosciences, Université Catholique de Louvain
Email: madina.samakbaeva@yandex.ru
Belgium, 1 Place L. Pasteur, Louvain-la-Neuve, 1348
A. Yu. Isaev
University of Tyumen
Email: madina.samakbaeva@yandex.ru
Russian Federation, 6 ul. Volodarskogo, Tyumen, 625003
D. A. Safin
Institute of Condensed Matter and Nanosciences, Université Catholique de Louvain; University of Tyumen
Email: madina.samakbaeva@yandex.ru
Belgium, 1 Place L. Pasteur, Louvain-la-Neuve, 1348; 6 ul. Volodarskogo, Tyumen, 625003
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