Condensation of СН-acids with  cis -1,4-dichlorobut-2-ene

G. Z. Raskildina; Yu. G. Borisova; E. A. Yakovenko; L. V. Spirikhin; S. S. Zlotskii

doi:10.1134/S1070363217010248

Condensation of СН-acids with cis-1,4-dichlorobut-2-ene

Authors: Raskildina G.Z.¹, Borisova Y.G.¹, Yakovenko E.A.¹, Spirikhin L.V.¹, Zlotskii S.S.¹
Affiliations:
1. Ufa State Petroleum Technological University
Issue: Vol 87, No 1 (2017)
Pages: 151-153
Section: Letters to the Editor
URL: https://journal-vniispk.ru/1070-3632/article/view/218079
DOI: https://doi.org/10.1134/S1070363217010248
ID: 218079

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Abstract

Synthesis of tri- and five-membered carboxylates are discussed. Microwave irradiation has been shown to stimulate the condensation of СН-acids with allyl chlorides. The selectivity of formation of target products was depending on the CH-acid structure. Structures of the isolated compounds have been confirmed by ¹Н and ¹³С NMR spectroscopy and chromato–mass spectrometry data.