(4-Methoxyphenyl)amine and its derivatives in the synthesis of  O -silylurethanes, ureas, and formamides

L. O. Belova; M. V. Pletneva; N. A. Golub; A. A. Korlyukov; A. D. Kirilin; A. V. Petrogradskii

doi:10.1134/S1070363217070143

(4-Methoxyphenyl)amine and its derivatives in the synthesis of O-silylurethanes, ureas, and formamides

Authors: Belova L.O.¹, Pletneva M.V.¹, Golub N.A.¹, Korlyukov A.A.¹, Kirilin A.D.¹, Petrogradskii A.V.¹
Affiliations:
1. Moscow Technological University (Institute of Fine Chemical Technologies)
Issue: Vol 87, No 7 (2017)
Pages: 1531-1535
Section: Article
URL: https://journal-vniispk.ru/1070-3632/article/view/220691
DOI: https://doi.org/10.1134/S1070363217070143
ID: 220691

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Abstract

Reactions of (4-methoxyphenyl)amine and its trimethylsilyl derivative with organosilicon isocyanates and phenylisocyanate have been studied. (4-Methoxyphenyl)formamide was first synthesized by the reaction of (4-methoxyphenyl)amine with ethyl formate. The structure of trimethylsilyl(4-methoxyphenyl)-carbamate and N-(4-methoxyphenyl)formamide was determined by X-ray diffraction (XRD) analysis.