One-pot synthesis of cage alcohols

Yu. N. Klimochkin; A. V. Yudashkin; E. O. Zhilkina; E. A. Ivleva; I. K. Moiseev; Ya. F. Oshis

doi:10.1134/S1070428017070028

One-pot synthesis of cage alcohols

Authors: Klimochkin Y.N.¹, Yudashkin A.V.¹, Zhilkina E.O.¹, Ivleva E.A.¹, Moiseev I.K.¹, Oshis Y.F.¹
Affiliations:
1. Samara State Technical University
Issue: Vol 53, No 7 (2017)
Pages: 971-976
Section: Article
URL: https://journal-vniispk.ru/1070-4280/article/view/216498
DOI: https://doi.org/10.1134/S1070428017070028
ID: 216498

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Abstract

An efficient one-pot procedure has been developed for the synthesis of cage alcohols with hydroxy groups in the bridgehead positions. The procedure includes initial nitroxylation with nitric acid or a mixture of nitric acid with acetic acid and subsequent hydrolysis in the presence of urea.