Synthesis of N-aryl- and  N , N -diethyl-9-methyl-11-sulfanylidene-8-oxa-10,12-diazatricyclo[7.3.1.0 2,7 ]trideca-2,4,6-triene-13-carboxamides

T. M. Zamaraeva; V. L. Gein; N. A. Buzmakova; M. V. Dmitriev

doi:10.1134/S1070428016070174

Synthesis of N-aryl- and N,N-diethyl-9-methyl-11-sulfanylidene-8-oxa-10,12-diazatricyclo[7.3.1.0^2,7]trideca-2,4,6-triene-13-carboxamides

作者: Zamaraeva T.M.¹, Gein V.L.¹, Buzmakova N.A.¹, Dmitriev M.V.²
隶属关系:
1. Perm State Pharmaceutical Academy
2. Perm State National Research University
期: 卷 52, 编号 7 (2016)
页面: 1022-1025
栏目: Article
URL: https://journal-vniispk.ru/1070-4280/article/view/214716
DOI: https://doi.org/10.1134/S1070428016070174
ID: 214716

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Three-component condensation of N-aryl- and N,N-diethyl-3-oxobutanamides with salicylaldehyde and thiourea in ethanol in the presence of sodium hydrogen sulfate afforded N-aryl- and N,N-diethyl-9-methyl-11-sulfanylidene-8-oxa-10,12-diazatricyclo[7.3.1.0^2,7]trideca-2,4,6-triene-13-carboxamides. Reaction of the same compounds in the absence of a catalyst under solvent-free conditions gave N-aryl-6-(2-hydroxyphenyl)-4-methyl-2-sulfanylidene-1,2,3,6-tetrahydropyrimidine-5-carboxamides.