电邮这篇文章 Sodium difluoromethanesulfinate—A difluoromethylating agent toward protonated heterocyclic bases
- 作者: Lytkina M.A.1,2, Eliseenkov E.V.2, Boyarskii V.P.2, Petrov A.A.2
-
隶属关系:
- St. Petersburg State Institute of Technology
- St. Petersburg State University
- 期: 卷 53, 编号 4 (2017)
- 页面: 539-546
- 栏目: Review
- URL: https://journal-vniispk.ru/1070-4280/article/view/216050
- DOI: https://doi.org/10.1134/S1070428017040066
- ID: 216050
如何引用文章
开放存取
##reader.subscriptionAccessGranted##
订阅存取
详细
Free radical difluoromethylation of protonated heteroaromatic bases was accomplished using sodium difluoromethanesulfinate in combination with tert-butyl hydroperoxide in a two-phase system (methylene chloride–water) at room temperature. The difluoromethylation products of methyl pyridine-4-carboxylate, pyridine-4-carbonitrile, and 2-amino-1,3,4-thiadiazole were isolated on a preparative scale.
作者简介
M. Lytkina
St. Petersburg State Institute of Technology; St. Petersburg State University
Email: aap1947@yandex.ru
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190005; Universitetskaya nab. 7/9, St. Petersburg, 190005
E. Eliseenkov
St. Petersburg State University
Email: aap1947@yandex.ru
俄罗斯联邦, Universitetskaya nab. 7/9, St. Petersburg, 190005
V. Boyarskii
St. Petersburg State University
Email: aap1947@yandex.ru
俄罗斯联邦, Universitetskaya nab. 7/9, St. Petersburg, 190005
A. Petrov
St. Petersburg State University
编辑信件的主要联系方式.
Email: aap1947@yandex.ru
俄罗斯联邦, Universitetskaya nab. 7/9, St. Petersburg, 190005
补充文件
