Oxidative Cyclization of Lithium 4-Ethoxy-1,1,1-trifluoro-4-oxobut-2-en-2-olate

N. S. Boltacheva; P. A. Slepukhin; V. I. Filyakova; V. N. Charushin

doi:10.1134/S1070428019060216

Oxidative Cyclization of Lithium 4-Ethoxy-1,1,1-trifluoro-4-oxobut-2-en-2-olate

作者: Boltacheva N.S.¹, Slepukhin P.A.¹, Filyakova V.I.¹, Charushin V.N.¹
隶属关系:
1. Postovskii Institute of Organic Synthesis, Ural Branch
期: 卷 55, 编号 6 (2019)
页面: 883-885
栏目: Short Communications
URL: https://journal-vniispk.ru/1070-4280/article/view/220798
DOI: https://doi.org/10.1134/S1070428019060216
ID: 220798

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详细

Diethyl 2,5-dihydroxy-2,5-bis(trifluoromethyl)tetrahydrofuran-3,4-dicarboxylate has been synthesized for the first time by reaction of lithium 4-ethoxy-1,1,1-trifluoro-4-oxobut-2-en-2-olate with manganese(III) acetate. The structure of its (2S*3S*4S*5S*) stereoisomer has been confirmed by X-ray analysis.