Synthesis of LaB6–ZrB2 Powder Mixture by Borothermal Reduction of La(OH)3 and ZrO(OH)2 Coprecipitated in Boron Suspension
- Авторы: Nesmelov D.D.1, Kozhevnikov O.A.1, Vikhman S.V.1, Novoselov E.S.1, Shatalkina I.V.1
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Учреждения:
- Prometei CRSI of Structural Materials, Kurchatov Institute SRC
- Выпуск: Том 60, № 4 (2019)
- Страницы: 389-393
- Раздел: Article
- URL: https://journal-vniispk.ru/1083-4877/article/view/249344
- DOI: https://doi.org/10.1007/s11148-019-00373-3
- ID: 249344
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Аннотация
Eutectic LaB6–ZrB2 powder was synthesized by borothermal reduction of an La(OH)3–ZrO(OH)2 mixture under vacuum with isothermal curing at 1200 – 1600°C. The mixture of hydroxides was prepared via coprecipitation from aqueous solutions of La and Zr nitrates in a suspension of amorphous boron. The effect of an excess of B on the phase and elemental compositions of the boride mixture was studied. The particle size of the obtained powders depended on the synthesis temperature.
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D. Nesmelov
Prometei CRSI of Structural Materials, Kurchatov Institute SRC
Автор, ответственный за переписку.
Email: dnesmelov@yandex.ru
Россия, St. Petersburg
O. Kozhevnikov
Prometei CRSI of Structural Materials, Kurchatov Institute SRC
Email: dnesmelov@yandex.ru
Россия, St. Petersburg
S. Vikhman
Prometei CRSI of Structural Materials, Kurchatov Institute SRC
Email: dnesmelov@yandex.ru
Россия, St. Petersburg
E. Novoselov
Prometei CRSI of Structural Materials, Kurchatov Institute SRC
Email: dnesmelov@yandex.ru
Россия, St. Petersburg
I. Shatalkina
Prometei CRSI of Structural Materials, Kurchatov Institute SRC
Email: dnesmelov@yandex.ru
Россия, St. Petersburg
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