


Vol 60, No 3 (2017)
- Year: 2017
- Articles: 27
- URL: https://journal-vniispk.ru/0020-4412/issue/view/9704
Nuclear Experimental Technique
The MPD test beam setup for testing detectors with the Nuclotron beams
Abstract
A new specialized MPD Test Beam setup was mounted at the extracted beam of the Nuclotron at the Joint Institute for Nuclear Research to carry out methodical research and test detectors produced for the MPD experiment at the NICA accelerating facility. The setup is described in detail. The results of the testing of fast detectors for the MPD time-of-flight system are presented as an example of the operation of the setup.



A high-voltage system of a differential spectrometer for measuring the neutron electric dipole moment
Abstract
A system of hardware and software for supplying a bipolar high voltage of up to 200 kV to a differential spectrometer that measures the neutron electric dipole moment is described. The high-voltage source is based on two 10-cascade voltage multipliers using quasi-resonant technology. The hardware and application software allow operation of the system in the manual, semi-automatic, and automatic modes.



Time characteristics of detectors based on silicon photomultipliers for the GlueX experiment
Abstract
Silicon photomultipliers (SiPMs) are used in detectors of the GlueX experiment devoted to studying the nature of confinement. These detectors are operable at counting rates as high as 2 MHz with a time resolution (FWHM) of approximately 0.3 ns and a number of excited pixels of up to 104. For SiPMs that operate under these conditions, the measured dependences of the recovery time and the time resolution are presented as functions of the number of excited pixels and the excitation frequency. Using a picosecond laser, the time resolution has been measured for an array of 4 × 4 SiPMs, which was specially developed for the experiment.



Investigation of a LYSO crystal for a low-energy calorimeter
Abstract
The results of studying a calorimeter cell in the low-energy region, ~50 MeV, which consists of a LYSO crystal and two avalanche photodiodes, are presented. The use of two photodiodes per crystal made it possible to perform a preliminary measurement of the calorimeter energy resolution using one calorimeter cell and cosmic muons. The coefficient of the stochastic contribution to the calorimeter energy resolution and the crystal luminescence time were measured (0.115% and 50 ns, respectively).



Laser photonics as a tool of experimental physics for recording and optical processing of particle tracks in track detectors
Abstract
Comparative results of recording and processing of particle tracks in track detectors by laser radiation with varying degrees of coherence are presented. The necessity to optimize the transformation parameter of the laser field coherence for each particular experimental task is substantiated.



Experimental investigations and mathematical simulation of the operation of ionizing-radiation diamond detectors
Abstract
A mathematical model of an ionizing-radiation monitor based on diamond detectors has been developed. Experimental investigations of the monitor were carried out, and, using their results, the model was verified and optimized. It was demonstrated that the developed model makes it possible to calculate data of sensor measurements with an accuracy of 10% or better. These results will be used to reconstruct cosmicradiation spectra according to the output data of the monitor.



Application of Computers in Experiments
A new control system for the capacitive energy storage of the GOL-3 multiple-mirror trap
Abstract
A new control system for capacitive energy storage with a rated energy content as high as 16 MJ is described. Capacitive energy storage has been used since 1987 to supply power for the pulsed magnetic system of the GOL-3 multiple-mirror trap. It has an operating voltage of 6 kV and consists of 6000 IK-6-150 capacitors that are located in six remote rooms together with the necessary infrastructure. The system for control and data acquisition was built using Arduino microcontroller boards operating as a distributed network of remote servers. The client part of the control system uses a personal computer with a standard configuration; communication with remote servers is effected by the TCP/IP protocol. The control system was put into regular operation at devices of the GOL-3 facility in the early 2016.



Electronics and Radio Engineering
A pulse method to estimate the efficiency of shielding magnetic fields
Abstract
A method for experimental evaluation of the magnetic-field attenuation coefficients under a pulsed action is considered. A technique for the preliminary processing of measurement results for low useful signal-to-noise ratios is considered taking the features of the operation of digital oscilloscopes into account. The analysis of the spectral composition of measured signals and a method for their approximation in the time domain, which allows elimination of the influence of measuring-sensor noise and digital-oscilloscope rounding errors, are presented. The results of estimating the frequency dependence of the magnetic-field attenuation coefficients for a copper shield in comparison with the results of a theoretical calculation are presented. The considered method allows simultaneous determination of the coefficients of the magnetic-field attenuation by the shield in a wide frequency range.



A generator of high-power nanosecond pulses based on a modular two-level summator
Abstract
A modular approach to designing generators of high-power high-voltage nanosecond pulses on the basis of a two-level wave summator and transistor formers of partial pulses is considered. The design and parameters of the modules that are oriented at the development of generators of voltage pulses of up to 300 kV at a current of up to 4 kA are described. The capabilities of these modules are demonstrated based on the example of a pulse generator with a power of 10 MW, a varied pulse duration of 50–150 ns, and a pulse repetition rate of up to 2 kHz.



An accelerating voltage generator for compact pulsed neutron sources
Abstract
A multistage generator of high-voltage pulses with a scroll geometry of spark switches, which is produced according to the Marx scheme, is presented. The device is designed for a small pulsed neutron source and makes it possible to obtain accelerating-voltage pulses with amplitudes of up to 450 kV at a stored energy of up to 50 J and a load current of up to 1.5 kA.



A microwave radiometer for deep noninvasive diagnostics of thermal fields inside a biological object
Abstract
A microwave radiometer for a wavelength of 10.5 cm with a frequency band of received signals of 200 MHz is described. It allows one to perform remote noninvasive temperature measurements deep in a biological object. The use of a modified null–reception method as the basis of the instrument operation made it possible to reduce the influence of the reflectance at the location of the contact between an applicator antenna and a body on the measurement accuracy and increase the dynamic characteristics during mapping of a biological object. At a storage signal time of 1 s, the measurement accuracy was 0.047 K. The output–signal changes were within 0.1 K when the reflectance was varied from 0.1 to 0.5.



General Experimental Techniques
Methods for investigating the spatial distribution of ion emission from micropinch-discharge plasma
Abstract
A technique for investigating the spatial structure of X-ray and ion-emission sources from micropinch- discharge plasma (MDP) is described and the investigation results are presented. A spectrometric system has been developed that allows measurements of the spectral characteristics of the ion emission for ions of different degrees of ionization from different MDP regions in a device of the low-inductance vacuum-spark type.



Pulsed field evaporation of ions from polar solutions
Abstract
An implementation of a technique for studying the release of ions from polar solutions under the action of electric field pulses is presented. A track membrane with nanoscale channels is used in this technique to stabilize the solution surface. The dependences of the ion yield on the parameters of extracting voltage pulses, as well as on the KI salt concentration in water−glycerol solutions have been obtained. The main advantage of the use of short pulses over a constant voltage technique is the possibility of expanding the range of the field strengths extracting ions from a solution without the risk that the solution leaks to the vacuum side of the membrane. In addition, a high stability of the extraction process is provided and the continuous operating time without membrane replacement is increased. The formation of the extraction field at the end of the channel due to the tip effect provides a fast start of the extraction process immediately after applying a voltage pulse, which also simplifies work with the membrane interface.



The installation to study the prebreakdown stage of a gas discharge by laser probing
Abstract
An installation to study a pulsed gas discharge in a diode with a single metal tip by laser probing has been devised. The installation represents a generator comprised of cable sections connected to a five-channel laser-triggered switch. The synchronization of the probing laser beam with the voltage pulse is not worse than ~1 ns. The moment of probing is determined by the optical delay and can be varied independently within the range of 10–20 ns by changing the charging voltage of the cables. The pressure in the discharge chamber can be varied from 10–5 Torr to atmospheric pressure. Copper or molybdenum wires with a diameter of 10 μm or greater were used as cathode pins. Three independent optical record channels with time delays of 2 and 13 ns relative to the first channel allow one to simultaneously obtain interferograms and shadow and schlieren images of the discharge gap with spatial and time resolutions of 20 μm and 70 ps, respectively, with the exposure time of each frame being equal to a laser pulse duration of 70 ps. Using the devised installation, qualitative and quantitative data on the prebreakdown processes that occur in a tip-type diode have been obtained within a wide range of pressures.



X-ray tomography as a diagnostic method of X-ray refractive optics
Abstract
This article describes the application of high-resolution X-ray computed tomography to assess the critical parameters of refractive lenses for X-ray optics that determine the quality of compound optical systems. A microfocus Y. Cheetah X-ray system has been used for three-dimensional visualization of the surface and internal structure of refractive lenses made of high-purity aluminum with geometric apertures of 500 and 1500 μm. A Fein Focus X-ray tube with a focal spot size of less than 2 μm provides the resolution necessary for detecting critical-size microstructure defects in the material of the lens.



An energy dispersion scheme based on a semiconductor X-ray spectrometer and a broadband monochromator for determining the content of heavy elements from the absorption spectra
Abstract
An energy-dispersion scheme for determining the conсentrations of impurities of heavy elements from the absorption spectra in the regions of X-ray photoabsorption jumps is described. A semiconductor X-ray spectrometer and a pyrolytic graphite monochromator were used to record data in a spectral band of width up to 1 keV. The initial shape of the absorption spectrum in the approximation of an isolated atom was reconstructed by means of a numerical solution of the convolution equation. The scheme provides a sharp increase in the data acquisition and measurement sensitivity. The results of measurements of the Bi and Pb contents in samples with organic matrices and determination of the thicknesses of thin Mo films on diamond substrates are presented.



An imaging spectroradiometry system for measuring spatial temperature distributions in microscopic objects
Abstract
An imaging-spectrometry method for measuring the spatial distributions of the temperature of microscopic objects with nonuniform spectral-emissivity distributions over their surfaces is described. An acousto-optic imaging spectrometer that allows measurements of the temperature distributions in the range of 500–5000 K with an error of ~1% and a spatial resolution of 500 × 500 elements over the surfaces of objects with dimensions of at most 5 mm was developed and manufactured. The efficiency of the instrument was demonstrated experimentally in measurements of the spatial distribution of the temperature of a laserheated tungsten plate.



Physical Instruments for Ecology, Medicine, and Biology
Development and research of a laser photo-acoustic SF6 gas analyzer
Abstract
An analysis of various optical schemes for the development of a laser SF6 gas analyzer based on a CO2 laser operating in free-running mode and a resonant photo-acoustic detector (PAD) is presented. The use of a sealed gas-filled cell to normalize PAD signals on the absorbed power in the cell is suggested. Compensation for the influence of the tuning of the CO2 laser wavelength near 10.6 μm on measured SF6 concentration is possible. The results of experimental studies of a laser photo-acoustic SF6 gas analyzer at various concentrations, including in the air flow, are presented. It is shown experimentally that the relative measurement error of the SF6 concentration due to the instability of the laser radiation wavelength does not exceed 5% in the range from ~80 ppb to 40 ppm. The limit of the sensitivity of the developed gas analyzer was ~1 ppb SF6.



Measurements of the nonlinear acoustic parameter of sea water via a device using reflected pulses
Abstract
A method for measuring the nonlinear acoustic parameter of sea water and a device in the form of an immersed sonde are described. The method is based on the principle of registration of waves at the difference frequencies in water at consecutive reflections of high-frequency biharmonic acoustic pumping waves between the walls of a measuring cell. Some results obtained during vertical sounding of the upper layer of the sea to a depth of 100 m are presented.



Laboratory Techniques
A particle-image velocimetry system for measurement of velocity flow fields for investigations of thermohydraulic processes on the large-scale benchmark of a promising fast-neutron reactor
Abstract
The use of visualization techniques in the research on thermohydraulic processes using large-scale models of nuclear power plants is discussed. In particular, the original particle-image velocimetry (PIV) measurement system at the TISEI test bench was presented, which is a model of a proposed fast-neutron reactor. Illumination and video-filming systems with the simultaneous use of several lasers and camcorders, as well as image-processing algorithms that make it possible to carry out field measurements with high precision in a complex configuration of the reactor model, reflections and distortions of the laser knife section, and shadowing by obstacles are described. The developed methodology of conversion of the image coordinates and velocity field into the reference system of the reactor model using a virtual 3D simulation made it possible to significantly simplify the experiments.



An atom probe tomography prototype with laser evaporation
Abstract
The results of development, creation, and tests of an atom-probe prototype with femtosecond laser evaporation and a position-sensitive microchannel detector with delay lines for the tomographic (3D) analysis of chemical composition of materials are presented. The atom-probe tomography is based on the principle of atom-by-atom “disassembling” of materials and projection magnification, which was previously used in field-ion microscopy, as well as the time-of-flight mass spectrometry that is applied to each evaporated ion. The prototype characteristics (mass resolution, spatial resolution, and data-collection efficiency) were demonstrated in study of tungsten.



Evaluation of the maximum size of through pores in MFAS-type membranes found by different methods
Abstract
Experiments to determine the maximum size of through pores in MFAS-type membranes (Vladipor Company) were carried out in two ways: by the “bubble-point” method according to GOST (State Standard) 50516-93 and the “crystallization-onset” method. The experimental values of the pressure difference upon the appearance of bubbles in a liquid and the temperature of the crystallization onset were obtained for membranes of different brands. It was shown that the membrane thickness influences these parameters. Repeated measurements of the maximum size of through pores were performed and showed good reproducibility of the experimental data.



Application of Jamin interferometer for the determination of thin transparent polymer films thickness in the visible range
Abstract
Modification of the technique for thickness determination of thin polymer films that are transparent in the visible range with the application of Jamin interferometer is suggested. The films are deposited on glass substrate. The technique is based on measuring the relative shift of interference fringes. The distinguishing feature of the approach is the use of three beams, one of which participates in the formation of the reference signal; the interference-fringe shift is estimated by the analysis of brightness curves.



A new method based on adaptive neuro-fuzzy inference system for determination of acid molarity using Compton scattered photons
Abstract
The simplicity and accuracy in determining the exact concentration of a particular substance in a solution, is one of the major issues in industrial chemistry. In this paper, we introduce a new technique based on Compton scattering of gamma photons and artificial intelligence to determine the concentration of a solute in a solution. We used a 137Cs gamma ray source with few millicurie activity and a NaI(Tl) scintillator detector to determine the acid sulfuric molarity. We also applied Adaptive Neuro-Fuzzy Inference System (ANFIS) and Artificial Neural Network (ANN) as artificial intelligence techniques to estimate the molarity of the samples. Monte Carlo simulations also support the present experimental results. The results of the proposed methods are in excellent agreement with the measured molarities.



High-speed vacuum evaporation of large-area targets by a focused electron beam
Abstract
A method of electron-beam evaporation of a target in a vacuum of ~10–2 Pa is considered. Initially, a focused electron beam spot moves at the periphery of the target in a circular path with an angular velocity of 8–80 rad/s by means of a ring sweep in the frequency range of 50–500 Hz. Then, by radial displacement with a linear velocity of 10–100 mm/s, the spot is guided over a spiral path from the edge of the target to its center. Due to spiral scanning, the spot runs across the entire target surface with a much larger area in 0.1–1.0 s and rapidly vaporizes the target.



A photodetector for the diagnostics of turbulent gas flows and flames by the method of absorption spectroscopy with diode lasers
Abstract
A photodetector device that is intended for absorption measurements at a level of 10–2–10–3 under the conditions of large intensity fluctuations of probing radiation, nonstationary broadband illumination of the photodetector, and in the presence of electromagnetic interference is described. Using a differential measurement circuit, an absorption signal is formed in the analog manner and amplified to a level of ~1 V directly near the photodetector. During periodic wavelength scanning, the influence of the broadband illumination and vibrations is compensated at the beginning of each scan. This compensation is preserved during a current scan and renewed in each subsequent scan due to the use of sample-and-hold amplifiers. The device can be used in the diagnostics of turbulent gas flows and flames.



An installation for studying luminescence excited by high-energy charged particles in dense xenon-containing gas mixtures with the possibility of regeneration and repeated use of xenon
Abstract
An installation for studying the spectral, temporal, and generation characteristics of xenon-containing high-pressure excimer mixtures is described. The mixtures are excited by a pulsed beam of fast electrons with energy Еe = 220 keV, pulse duration Тp = 5 ns, and maximum beam current density Imax = 20 A/cm2. Spectral and temporal measurements are taken in the wavelength range of 200–1200 nm with a wavelength resolution of 1 nm (the Maya-2000Pro spectrometer) and a temporal resolution of 2 ns/cm (a Tektronics TDS1024 oscilloscope and a FEU-106 photomultiplier tube). To reduce the xenon consumption when carrying out experimental investigations, the installation is equipped with a system of xenon peeling and regeneration, which allows the xenon loss to be reduced by factors of 50–100. The use of one additional external mirror for determining the gain characteristics of high-pressure excimer mixtures upon pumping with fast charged particles is considered.


