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Vol 58, No 5-6 (2016)

Article

Study of Microstructure Formation of Carbon Steel Under High-Speed and Multicycle Hot Plastic Compressive Deformation Using A Gleeble 3500 Unit

Koptseva N.V., Nikitenko O.A., Efimova Y.Y.

Abstract

Features of deformation regimes and mechanisms of microstructure formation in low-carbon steel 20 are studied using high-speed and multicycle hot plastic deformation methods in a Gleeble 3500 unit. Energy-force and temperature-speed regimes are established providing preparation of an ultrafine-grained structure with grain size of 150 – 1250 nm, similar to that achieved with higher degrees of cold plastic deformation. Specimen microhardness is determined.

Metal Science and Heat Treatment. 2016;58(5-6):318-323
pages 318-323 views

Study of Secondary Phase Particle Dissolution and Austenite Grain Growth on Heating Fine-Grained High-Strength IF-Steel

Jia H., Zhang H., Sun C.

Abstract

Dissolution of particles of second phase and growth of austenite grains in high-strength fine-grained IF-steel (0.0057% C, 0.0023% N) on heating is studied. Metallographic analysis of flat steel specimens cut from plates prepared by hot and cold rolling is performed. Steel structure is studied after holding for 10 – 60 min at different temperatures and water quenching. The quenching parameters at which the microalloying elements (Ti, Nb) dissolve completely with retention of fine-grained austenite are determined. Amathematical model of austenite grain growth is developed by nonlinear regression analysis of experimental data.

Metal Science and Heat Treatment. 2016;58(5-6):324-329
pages 324-329 views

Study of the Effect of Trace Mg Additions on Carbides in Die Steel H13

Li J., Li J., Wang L., Zhu Q.

Abstract

Carbides in annealed steel H13 without magnesium and with a micro-addition of magnesium (0.0010%) are studied. Trace amounts of magnesium strengthen carbide segregation and reduce their size. Carbides phases M7C3, M6 C, and M(C, N) are detected in steel H13, and this agrees with results of thermodynamic calculations.

Metal Science and Heat Treatment. 2016;58(5-6):330-334
pages 330-334 views

Effect of Gas-Saturated Layers on Titanium Alloy Sheet Mechanical Properties

Kolomenskii A.B., Shakhov S.V., Kolomenskii B.A.

Abstract

The effect of the thickness of gas-saturated layer and annealing temperature on impact strength of titanium alloys is studied. It is shown that the optimum degree of the surface gas saturation may have a favorable effect on titanium alloy sheet endurance and impact strength.

Metal Science and Heat Treatment. 2016;58(5-6):340-345
pages 340-345 views

Structure and Properties of High-Strength Aluminum Alloy 1933 Rolled Plates

Selivanov A.A., Vakhromov R.O., Setyukov O.A., Popova O.I.

Abstract

Results are given for metallographic and x-ray diffraction analysis of the structure, degree of recrystallization, and preferred crystallographic orientations, and also mechanical and corrosion properties through the thickness of 100 mm thick rolled plates of high-strength aluminum alloy 1933, considered in this study as an alternative to forgings.

Metal Science and Heat Treatment. 2016;58(5-6):352-356
pages 352-356 views

Effect of Magnesium Additions on Composites with Al and Al – 12% Si Matrices Strengthened with B4C and Prepared by Infiltration Under Pressure

Çevik E., Sun Y., Ahlatci H., Turen Y.

Abstract

Metallographic and x-ray phase analyses are used for metal-matrix composites Al – B4C and (Al – 12% Si) – B4C with a volume fraction of 60% boron carbide prepared by infiltrating a pressed workpiece with metal under pressure. It is shown that with introduction of 1 to 4% Mg into a metal matrix composite porosity is reduced from 7 to 1%.

Metal Science and Heat Treatment. 2016;58(5-6):357-361
pages 357-361 views

Effect of Carbonitriding in a Salt Bath by a QPQ Scheme on Stainless Steel 321 Microstructure and Service Properties

Bellas L., Castro G., Mera L., Mier J.L., García A., Varela A.

Abstract

Wear resistance, corrosion properties and structure of reinforced layers deposited on steel AISI 321 with carbonitriding by the quench-polish-quench (QPQ) Tennifer® process with subsequent oxidation are studied. The structure of the layers is investigated by scanning electron microscopy with energy dispersive local analysis and x-ray diffractometry. Steel wear resistance is determined by a pin-on disk test, and oxide layer adhesion is determined by a scratch method. Pitting corrosion resistance is determined by plotting cyclic polarization curves.

Metal Science and Heat Treatment. 2016;58(5-6):369-375
pages 369-375 views

Features of Intermetallic Alloy TNM-B1 High-Temperature Oxidation

Smyslov A.M., Bybin A.A., Dautov S.S.

Abstract

Features of intermetallic alloy based on titanium aluminide high-temperature oxidation at 800 – 850°C are studied. A mathematical dependence is obtained for oxidation rate on test duration. The structure and composition of an oxide layer formed during high-temperature oxidation are studied. It is shown that under operating conditions at the maximum working temperatures the intermetallic alloy exhibits low heat resistance.

Metal Science and Heat Treatment. 2016;58(5-6):268-272
pages 268-272 views

Precipitation Hardening of Laser-Surfaced Layer of Maraging Alloy at the Surface of Steel 3Kh3M3F

Stavrev D.S., Shcherbakov V.S.

Abstract

The structure and fracture behavior of a layer of maraging alloy deposited by laser surfacing on steel 3Kh3M3F is studied in the initial condition and after precipitation hardening at 550 and 600°C. Microhardness is measured in layer cross sections, and fractures after surfacing and aging are analyzed in an electron microscope.

Metal Science and Heat Treatment. 2016;58(5-6):376-379
pages 376-379 views

Study of Alloy Microstructure Based on TiNi After High-Temperature Treatment

Senkevich K.S., Gusev D.E.

Abstract

Features of microstructure formation for alloy based on titanium nickelide after high-temperature treatment at 1050 – 1250°C are studied. Heat treatment conditions are stipulated diffusion welding and sintering regimes developed previously for alloys based on TiNi.

Metal Science and Heat Treatment. 2016;58(5-6):273-278
pages 273-278 views

Effect of Artificial Aging on the Microstructure and Mechanical Properties of Aluminum Alloy AA6061-T6

Toozandehjani M., Mustapha F., Ariffin M.K., Zahari N.I., Matori K.A., Ostovan F., Fadaeifard F.

Abstract

The properties of aluminum alloy AA6061-T6 after aging at 220°C for 0.5 – 8 h are studied by the methods of light and scanning electron microscopy and fractography. The mechanical characteristics of the alloy are determined by tensile tests.

Metal Science and Heat Treatment. 2016;58(5-6):283-286
pages 283-286 views

Nomograms to Determine the Controlling Factors in Vacuum-Carburizing Regimes

Semenov M.Y.

Abstract

A method based on computer evaluation of mechanical properties and a mathematical model of vacuum carburizing are used for creating two nomograms, i.e., (1 ) for determining the parameters that the carburized layers of gears of steel 16Kh3NVFMB-Sh must have to obtain the required service properties and (2 ) for determining the values that the factors in periodic carburizing regimes must have to ensure that the layers have the prescribed parameters. The nomograms are used to determine the factors for two gears that are to undergo vacuum carburizing.

Metal Science and Heat Treatment. 2016;58(5-6):293-298
pages 293-298 views

Diagnostics of the Properties of Steel Articles According to the Criterion of Microhardness

Astashchenko V.I., Shveev A.I., Shveeva T.V.

Abstract

On the basis of metallographic monitoring of semimanufactured steel pieces and automobile parts, it is shown that prediction of the properties of articles on the basis of the criterion of microhardness of individual structural constituents and the difference in the values of the criterion represents an effective approach.

Metal Science and Heat Treatment. 2016;58(5-6):303-307
pages 303-307 views

Promising Versions of α-Martensite Rod-Like Crystal Initiation in Iron Alloys by Three Elastic Wave Sources

Kashchenko M.P., Chashchina V.G.

Abstract

Versions are provided for α-martensite rod-shaped crystal initiation by three orthogonal longitudinal elastic waves propagating in orthogonal directions of the types 〈001〉γ and 〈110〉γ in Fe – 31% Ni single crystals. The probability is considered of direct initiation by Bain-type deformation waves. It is demonstrated within the scope of dynamic theory that the anticipated orientation of rod-like crystals is close to 〈111〉γ or to 〈905〉γ. Possible features of martensite crystal tetragonality are discussed. Ultrasound source power required for initiating martensitic transformation is determined.

Metal Science and Heat Treatment. 2016;58(5-6):254-258
pages 254-258 views

Titanium Alloys

Features of Titanium Structure Formation During Thermal Diffusion Saturation with Hydrogen

Kollerov M.Y., Mamonov A.M., Zasypkin V.V., Spektor V.S., Runova Y.É.

Abstract

Some features are provide for the change in structure and properties of commercial purity titanium during hydrogenation and their effect on formation of the final structure of semifinished products and objects after vacuum annealing. It is established that titanium hydrogenation kinetics by a thermal diffusion method and specimen structure formation are mainly determined by the temperature for introducing hydrogen.

Metal Science and Heat Treatment. 2016;58(5-6):335-339
pages 335-339 views

Thermodynamic Modeling and Experimental Study of Phase Transformations in Alloys Based on γ-TiAl

Kuznetsov A.V., Sokolovskii V.S., Salishchev G.A., Belov N.A., Nochovnaya N.A.

Abstract

Thermo-Calc software is used to model the composition diagram for alloys based on γ-TiAl of the systems Ti – Al – Mo – (4 – 10) at.% Nb and Ti – Al – Nb – X (X is Cr, Mo, V). The effect of alloying on critical points and sequence of phase transformations is established. Changes in phase composition in relation to alloy TNM-B1 temperature are analyzed using a polythermal section of the Ti – Al – Nb – Mo system.

Metal Science and Heat Treatment. 2016;58(5-6):259-267
pages 259-267 views

Aluminum Alloys

Structure and Properties of Thick-Walled Joints of Alloy 1570s Prepared by Friction Stir Welding

Velichko O.V., Ivanov S.Y., Karkhin V.A., Lopota V.A., Makhin I.D.

Abstract

The microstructure and mechanical properties of thick-walled joints of Al – Mg – Sc alloy 1570S, prepared by friction stir welding are studied. Joint microstructural and mechanical inhomogeneity are revealed.

Metal Science and Heat Treatment. 2016;58(5-6):346-351
pages 346-351 views

Effect of Crystal Structure Fineness for Charge Alloy AK6M2 on Its Flux Treatment Efficiency

Nikitin K.V., Nikitin V.I., Timoshkin I.Y., Chikova O.A.

Abstract

The effect of charge billet structure and form of fluxes on structure, density, and gas content of alloy AK6M2 (Al – Si – Cu system) is studied. Alloys prepared from finely crystalline charge billet have smaller phase component sizes, lower gas content, and increased solid state density, and use of coarsely crystalline charge billets for alloy preparation necessitates an increase in flux preparation consumption in the stage of alloy preparation for casting.

Metal Science and Heat Treatment. 2016;58(5-6):279-282
pages 279-282 views

Treatment

Two-Stage Heat Treatment of Steel 30CrMnSi and Its Optimization

Nekouei R.K., Akhaghi R., Tahmasebi R., Ravanbakhsh A., Moghaddam A.J.

Abstract

The effect of cooling medium on the microstructure and mechanical properties of steel 30CrMnSi is studied after different heat treatment. Microstructure is studied by scanning electron microscopy, energy dispersion analysis, and fractography. Impact strength, shear punch stress, friction coefficient, and wear resistance in pin-on-disk tests are determined. Phase transformations with tempering are studied by dilatometry. A heat treatment regime providing an optimum set of steel properties is proposed.

Metal Science and Heat Treatment. 2016;58(5-6):362-368
pages 362-368 views

Thermochemical Treatment

Special Features of the Carbonitriding of Parts of Instrument Bearings Designed for Extreme Service Conditions

Smirnov A.E., Shevchenko S.Y., Shchipunov V.S., Kunyaev V.E., Seval’nev G.S.

Abstract

A study is made of complexly alloyed steel 8Kh4V9F2-Sh, which is used for fabricating parts of engineering bearings operating under extreme conditions. Vacuum processes are shown to be preferable to gas carburizing for hardening the races of precision bearings. Vacuum carburizing is shown to be an effective technique for forming quality diffusion layers.

Metal Science and Heat Treatment. 2016;58(5-6):287-292
pages 287-292 views

Technical Information

Technologies for Use in the Formation of a Differentiated Structure in Iron Billets Used in Glass Molds

Leushin I.O., Chistyakov D.G.

Abstract

Causes for the failure of pig iron press molds that are parts of a glass mold are described. Criteria for differentiating the structure of pig iron are established. Ways of obtaining a differentiated structure of a casting product are outlined. A heat treatment regime for the billets is determined.

Metal Science and Heat Treatment. 2016;58(5-6):299-302
pages 299-302 views

Transformations

Effect of External Actions and a Magnetic Field on Martensitic Transformation in Steels and Alloys

Schastlivtsev V.M., Kaletina Y.V., Fokina E.A., Mirzaev D.A.

Abstract

The historical aspect is provided for research into the effect of a magnetic field and a number of other actions on martensitic transformation in steels and alloys.

Metal Science and Heat Treatment. 2016;58(5-6):247-253
pages 247-253 views

Structural and Die Steels

Structural and Magnetic Stability of Austenite in Chromium-Nickel and Manganese Steels with Cold Deformation

Ol’shanetskii V.E., Snezhnoi G.V., Sazhnev V.N.

Abstract

Chromium-nickel and high-manganese steels are studied. The specific magnetic susceptibility χ0 of paramagnetic austenite is shown by experiment to depend on nickel content in chromium-nickel steels and on manganese in manganese steels subjected to compressive deformation. It is shown that with an increase in nickel content, apart from structural stabilization of austenite, there is an increase in χ0. The effect of manganese on parameter χ0 in manganese steels is the opposite. Localized distribution of Cr and Ni elements and presence of regions of a ferromagnetic phase at austenite grain boundaries in chromium-nickel steels is revealed.

Metal Science and Heat Treatment. 2016;58(5-6):311-317
pages 311-317 views