Effect of crystallization annealing under loading on the magnetic properties and the structure of a soft magnetic FeSiNbCuB alloy doped with chromium

Resumo

The changes of quasi-static magnetic hysteresis loops and X-ray diffraction patterns of the Fe_73.5Si_13.5B₉Nb₃Cu₁ doped to 10 at % chromium instead of iron have been studied to elucidate the influence of the thermomechanical treatment consisting of annealing and cooling of the alloy under the tensile stress (tensile-stress annealing (TSA)) on the magnetic properties and the structure of these alloys. It is shown that the treatment results in the induction of the magnetic anisotropy of the hard axis type at which the magnetization reversal along the direction of applying the external stress during annealing is hampered. The energy of the induced magnetic anisotropy decreases as the chromium content increases. During TSA, the nanocrystal lattices are deformed, and the deformation is retained after cooling. The interplanar spacings increase along the extension direction and decrease in the transverse direction. The deformation anisotropy is observed for crystallographic directions. The anisotropic deformation of the bcc lattice of nanocrystals with high content of the ordered Fe₃Si phase characterized by a negative magnetoelastic interaction is the cause of formation of the state with the transverse magnetic anisotropy of the hard axis type.