Fabrication and physicochemical characterization of graphene oxide derived from thermally expanded graphite


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Graphene oxide was obtained from expanded graphite according to the modified Hummers method. The reaction time was significantly reduced (from 24 to 8 h) by applying the expanded graphite in the oxidation process. The interlayer distance in obtained samples was equal to 0.70–0.74 nm. Structural features of the material were studied by the powder X-ray diffraction, thermogravimetric analysis, scanning electron microscopy, transmission electron microscopy, XPS spectroscopy, and NMR spectroscopy.

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L. Ilkevich

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

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Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

T. Tkachenko

Kemerovo State University

Email: lida1193@mail.ru
俄罗斯联邦, 6 ul. Krasnaya, Kemerovo, 650043

A. Samarov

Department of Chemistry, M. V. Lomonosov Moscow State University

Email: lida1193@mail.ru
俄罗斯联邦, Build. 9, 1 Leninskie Gory, Moscow, 119991

A. Burtsev

Department of Chemistry, M. V. Lomonosov Moscow State University

Email: lida1193@mail.ru
俄罗斯联邦, Build. 9, 1 Leninskie Gory, Moscow, 119991

S. Sozinov

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

L. Hitsova

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

A. Popova

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

Ch. Barnakov

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

A. Kozlov

Federal Research Center for Coal and Coal Chemistry, Siberian Branch of the Russian Academy of Sciences

Email: lida1193@mail.ru
俄罗斯联邦, 18 Sovetskiy prosp., Kemerovo, 650000

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