


Vol 42, No 5 (2016)
- Year: 2016
- Articles: 30
- URL: https://journal-vniispk.ru/1063-7850/issue/view/12428
Article
The effect of heating rate on thermoluminescence of anion-defective alumina after high-dose irradiation
Abstract
The dependences of the light sum of peaks of thermoluminescence (TL) at 180 and 300°C on the rate of heating of single crystals of anion-defective alumina after high-dose irradiation are investigated. It is found that these dependences for the peak at 180°C are the same for all studied samples and match the known dependence measured after low-dose irradiation. The curves for the TL peak at 300°C vary significantly from one sample to another. The parameters of thermal TL quenching are calculated for both peaks using the Monte Carlo method. Practical suggestions regarding the use of the obtained results in high-dose dosimetry are provided.



A lens acoustic microscope with a two-dimensional ultrasound array
Abstract
A lens acoustic microscope is proposed in which a two-dimensional high-frequency ultrasound array is used instead of a single converter. In this microscope, electronic scanning of the region of naturally occurring focus of the acoustic lens can be performed and the focus can be held electronically at different distances, including inside solid objects. It was demonstrated that the multielement microscope has potentially higher performance compared with a single-element scanning microscope and is not inferior in resolution power.



The effect of working gas pressure on the switching rate of a kivotron
Abstract
The switching rate in gas-discharge devices (kivotrons) based on an “open” discharge with counterpropagating electron beams is studied experimentally. Structures with a total cathode area of 2 cm2 were used. A monotonic reduction in the switching time with an increase in the working gas pressure and in the voltage amplitude at the time of breakdown is demonstrated. The minimum switching time is ~240 ps at a voltage of 17 kV. The maximum current rise rate, which is limited by the discharge circuit inductance, is 3 × 1012 A/s.



Excitation of hypersound by multiplication of the ferromagnetic resonance frequency in a magnetostriction transducer
Abstract
With reference to the problem of increasing the frequency of hypersound excited by a magnetostriction transducer, the feasibility of multiplication of the frequency by multiplication of the eigenfrequency of the elastic resonator is considered. It is shown that efficient multiplication is possible only in odd harmonics of the excitation signal. For interpretation of the phenomenon observed, a model of nonlinear excitation due to multiplication of the values of the longitudinal and transverse magnetization components is proposed.



The influence of thermophysical properties of an anisotropic heat-element substrate on the value of thermal emf in the stationary thermal mode
Abstract
Thermal and thermoelectric processes in anisotropic heat elements located on substrates made of different materials have been numerically simulated. It is shown that, when an invariable heat flux passes through a heat element, the thermophysical properties of the substrate and heat transfer coefficient at its rear surface affect significantly the temperature distribution and the value of generated thermal emf.



Complex use of the diffraction techniques in depth profiling of the crystal lattice parameter and composition of InGaAs/GaAs gradient layers
Abstract
A technique is proposed for testing thick (1 μm and larger) gradient layers with the composition and relaxation degree alternating over the layer depth on the basis of comparative analysis of X-ray scattered intensity maps in the reciprocal space and depth profiles of the crystal lattice parameters obtained by electron microdiffraction. The informativity of the proposed technique is demonstrated using the example of an InxGa1–xAs/GaAs layer with linear depth variation in x. Complex representation of the diffraction data in the form of the depth-profiled reciprocal space map allows taking into account the additional relaxation caused by thinning electron microscopy specimens.



The formation of ZnO-based coatings from solutions containing high-molecular polyvinylpyrrolidone
Abstract
A method for deposition of transparent nanosize ZnO-based coatings on the glass surface from solutions containing high-molecular polyvinylpyrrolidone is described. The method can be used to form transparent homogeneous coatings based on ZnO with an increased energy gap width. It does not require any intricate technological equipment.



Determination of topological parameters of a laser with passive mode-locking on the basis of InGaAlAs/InGaAs/InP heterostructures
Abstract
Topological parameters of a strip-geometry laser with passive mode-locking on the basis of an InGaAlAs/InGaAs/InP heterostructure are determined from the condition for the existence of one transverse mode in a strip waveguide. The strip width was 1.5 μm, the mesa etch depth was 1.32 μm, and the thickness of the dielectric layer was 0.36 μm.



A method and apparatus for high-throughput controlled synthesis of fullerenes and endohedral metal fullerenes
Abstract
A method for synthesis of carbon nanostructures in a high-frequency arc discharge in the flow of helium (3–4 L/min) is presented. It is shown that the plasma-chemical synthesis of fullerenes and endohedral metal fullerenes (EMFs) can be controlled by changing helium pressure in the chamber. Temperature and electron concentration along the line normal to the discharge axis decrease upon moving away from the axis to the periphery; the larger the pressure, the sharper is the decrease in these parameters. The optimal helium pressure of 98 kPa was found in obtaining the Gd@C82 EMF which corresponds to the maximal EMF yield of 5 wt %.



Microfluidic chips for the study of cell migration under the effect of chemicals
Abstract
Numerical simulation of the formation of a chemoattractant gradient in reaction chambers of a chip having different geometries enabled the determination of a structure suitable for the study of cell migration, in accordance with which hybrid polymer–glass microfluidic devices were manufactured. Verification of the procedures of alignment of cells in the reaction chamber of the chip by centrifugal force and subsequent culturing of the cells showed that microfluidic chips can be used to study cell migration under the effect of the chemoattractant gradient in vitro.



Electrochemical etching of p–n-GaN/AlGaN photoelectrodes
Abstract
Specific features of etching of GaN/AlGaN p–n structures in a KOH-based electrolyte have been studied. It was found that the corrosion process first passes across p layers through vertical channels associated with threading structural defects. Then, the corrosion process occurs in the lateral direction along n layers of the structure, with local hollows and voids thereby formed. The lateral etching is due to the presence of positive piezoelectric charges at boundaries of n-AlGaN and n-GaN layers and positively charged ionized donors in the space-charge region of the p–n junction.



The influence of a metal on transverse characteristics of hybrid waves in a layered ferrite–ferroelectric structure
Abstract
We present electrodynamic characteristics of a layered multiferroic structure of metal–dielectric–ferrite–dielectric–ferroelectric–dielectric–metal type calculated by the finite elements method. Properties of transverse modes of hybrid waves (dispersion characteristics, electric field distribution at different frequencies, and damping rate) as functions of the distance between the ferroelectric layer and the metal screen are analyzed for the first time.



Nitriding of stainless steel in plasma of a pulse electron beam
Abstract
The formation of a hardened layer with low-temperature (400°C)nitriding of grade 12Kh18N10T stainless steel in plasma of a pulse electron beam which is generated under continuous and pulse conditions at equal average current (2.6 A) and electron energy (200 eV) is studied. In spite of intense ion sputtering of the surface during the pulse, both nitriding conditions yielded equal quantities of thickness and hardness of the layer, which indicated that neutral atomic nitrogen plays a main role during nitriding.



Peculiarities of metal oxide nanoparticles obtained in acoustoplasma discharge
Abstract
Nanoparticles of tungsten, copper, iron, and zinc oxides were synthesized in acoustoplasma discharge. Their size distribution was studied by electron microscopy and laser correlation spectroscopy. Ultrasound was found to narrow significantly the size distribution width of zinc oxide nanoparticles. Water suspensions of zinc oxide nanoparticles showed photoluminescence in red and near infrared spectral ranges, which makes them a promising material for luminescent diagnostics of biological systems.



The photosensitivity of ytterbium-doped optical fibers with aluminophosphosilicate glass cores
Abstract
The phenomenon of photoinduced refractive index change in active optical fibers with Al2O3/P2O5/Yb2O3/SiO2 core composition has been observed under the action of UV laser radiation with 193-nm wavelength. It is established that hydrogen treatment of active fibers plays a key role in ensuring a radical (about two orders of magnitude) increase in their photosensitivity. It is shown that intrafiber Bragg gratings with reflection coefficients above 99% can be formed, which are promising mirror reflectors for fiber laser cavities.



A fiber-optic frequency transducer of variable pressure in gaseous and liquid media
Abstract
Fiber-optic sensors of variable pressure are proposed and implemented on fiber lasers with microoptomechanical resonance structures generating in automodulation regimes. Possibilities of sound pressure monitoring in gaseous and liquid media are considered, and the sensitivity of these fiber-optic sensors is estimated.



Resistive switching in Au/SiOx/TiN/Ti memristive structures with varied geometric parameters and stoichiometry of dielectric film
Abstract
We have studied Au/SiOx/TiN/Ti memristive structures obtained by magnetron sputtering, which exhibit a reproducible resistive switching effect. The influence of the thickness and stoichiometry of SiOx layer and the area of Au electrode on the parameters of switching has been analyzed. The obtained results show evidence in favor of the filament model of resistive switching in SiOx films.



A planar diamond-like carbon nanostructure for a low-voltage field emission cathode with a developed surface
Abstract
Issues pertaining to the effective solution of problems related to the creation of durable low-voltage field emission cathodes with developed working surface and high density of emission current are considered. Results of practical implementation of the concept of multielectrode field emission planar nanostructures based on diamond-like carbon are presented. High average current density (0.1–0.3 A cm–2) is ensured by the formation of a controlled zone of electrostatic field localization at the planar-edge structure. The working life of cathode samples reaches 700–3000 h due to several positive factors, such as the stabilizing properties of a diamond-like carbon film, protection of the emitter from ion bombardment, use of a system of ballast resistors, and low-voltage operation of submicron interelectrode gaps.



Polarization separation in titanium-diffused waveguides on lithium niobate substrates
Abstract
The influence of technological parameters of the process of thermal diffusion of titanium in lithium niobate substrates on the polarization-dependent losses of obtained optical waveguide has been theoretically studied. It is established that the anisotropy of refractive index variation leads to different conditions of polarization eigenmode cutoff that can be used for separating extraordinary and quenching ordinary polarization modes. Experiments with titanium-diffused waveguides showed the possibility of extraordinary polarization mode separation above 40 dB in the C-range (1530–1565 nm) of telecommunication wavelengths.



Pyrolytic deposition of nanostructured titanium carbide coatings on the surface of multiwalled carbon nanotubes
Abstract
Nanostructured titanium carbide coatings have been deposited on the surface of multiwalled carbon nanotubes (MWCNTs) by the MOCVD method with bis(cyclopentadienyl)titanium dichloride precursor. The obtained TiC/MWCNT hybrid materials were characterized by X-ray diffraction, scanning electron microscopy, and high-resolution transmission electron microscopy. It is established that a TiC coating deposits onto the MWCNT surface with the formation of a core–shell (MWSNT–TiC) type structure.



A high-sensitivity scanning magnetometer based on the giant magneto-impedance effect for measuring local magnetic fields of corrosion currents
Abstract
The design, main characteristics, and specific features of a new high-sensitivity magnetometer based on the giant magneto-impedance (GMI) effect in amorphous ferromagnetic microwires are considered. It is shown that, in addition to measuring homogeneous fields, the device is capable of detecting weak local magnetic fields of conduction currents and ion currents involved in corrosion processes. Results of in situ magnetic measurements of corrosion processes in the model system of copper–zinc in a sulfuric acid solution qualitatively agree with the data of direct corrosion tests employing the standard gravimetric method.



An experimental study of freezing of supercooled water droplet on solid surface
Abstract
Results of experimental investigations of the freezing of immobile water droplet on an aluminum plate are presented. The process was studied with the aid of a high-speed photo camera. The freezing of supercooled water contained in the surface droplet proceeds in a few stages: (i) preliminary heating of water and nucleation of ice microcrystals, (ii) relatively fast formation of the ice–liquid system with a transition to the state of thermodynamic equilibrium near the freezing temperature, and (iii) slow process of complete freezing. The rate and duration of each stage and the time of delay between the moment of action upon the supercooled droplet and the onset of freezing are estimated. Processes of supercooled and nonsupercooled water solidification are compared.



Influence of ion energies on the structure, composition, and properties of multilayer Ti–Al–Si–N ion-plasma-deposited coatings
Abstract
It is established that the energy of deposited particles influences the structure, composition, and properties of multilayer nitride coatings consisting of alternating layers of nanocrystalline TiN and amorphous Si3N4 phases with inclusions of nanocrystalline hexagonal AlN formed at energies of titanium, aluminum, and silicon ions exceeding ~317 × 10–19, 267 × 10–19, and 230 × 10–19 J, respectively. As the energy of titanium ions bombarding the substrate increases above ~512 × 10–19 J, the phase transition from disordered TiNx to Ti3N2 and the appearance of 2- to 3-nm-thick sublayers in 15-nm-thick nanocrystalline TiNx layers take place in the coating. The maximum hardness of such coatings reaches a level of ~54 GPa.



Structure engineering in vacuum-arc-deposited coatings of the MoN–CrN system
Abstract
The possibilities of structure engineering in multilayer coatings of the MoN–CrN system with relatively low heats of formation of component transition metal nitrides are demonstrated by varying pressure PN of reactive gas (nitrogen) and negative bias voltage–Us applied to a metal substrate. It is established that, by changing PN from 7 × 10–4 to 3 × 10–3 Torr, it is possible to obtain coatings in two significantly different structural-phase states. A multilayer nonisostructural composite with hexagonal crystalline lattice in CrN layers and cubic type lattice in MoN layers is formed at low pressure, whereas an isostructural state with cubic lattice in both nitride layers is formed at high pressure. The existence of two types of structural states allows multilayer coatings with controlled hardness to be obtained, which reaches 38 GPa in the isostructural state.



Light-induced resistive switching in silicon-based metal–insulator–semiconductor structures
Abstract
We have studied light-induced resistive switching in metal–insulator–semiconductor structures based on silicon covered with a tunneling-thin SiO2 layer and nanometer-thick layer of antimony. The role of an insulator was played by yttria-stabilized zirconia.



Semi-insulating GaN:C epilayers grown by metalorganic vapor phase epitaxy using propane as a carbon source
Abstract
The influence of propane present in a reactor at various stages of GaN growth by metalorganic vapor phase epitaxy (MOVPE) on sapphire substrates on the character of epitaxial process and the properties of epilayers has been studied. Doped GaN epilayers with carbon concentration 5 × 1018 cm–3 characterized by high crystalline perfection, an atomically smooth surface, and electric breakdown voltage above 500 V at a doped layer thickness of 4 μm have been obtained.



Experimental investigation of electron guns for THz microwave vacuum amplifiers
Abstract
Single-sheet and multiple beam electron emitters based on thermionic minicathodes for terahertz traveling-wave tubes have been studied. Data are presented for impregnated blade thermionic cathode with dimensions 0.1 × 0.7 mm and a maximum current density of 114 A/cm2 in a pulsed mode. A variant of the five-beam electron gun with 0.25-mm-diameter cylindrical minicathodes in cells of a control grid is proposed that provides a current density of 85.5 A/cm2 at a grid potential of 900–1000 V.



Shape-coupled magnetoresistive structures: a new approach to higher sensitivity
Abstract
A new type of anisotropic magnetoresistive structures is proposed in which the shape of ferromagnetic elements repeats the shape of nonmagnetic conducting shunts. The results of numerical simulations with allowance for inhomogeneous magnetization distribution showed that these shape-coupled structures exhibit a significant (~70%) increase in sensitivity as compared to that of classical barber-pole structures.



The defect mode in a low-dimensional waveguide microwave photonic crystal
Abstract
It is shown that the violation of periodicity in a low-dimensional waveguide microwave photonic crystal, in which the periodic structure is formed by dielectric layers and adjacent metal plates partly overlapping the waveguide cross section and forming capacitive gaps between the plate edge and wide wall of the waveguide, leads to the appearance of a defect (impurity) mode. It is established that the defect mode position on the frequency scale significantly depends on both the thickness of “disturbed” dielectric layer and the capacitive gap width of diaphragms.



Erratum
Erratum to: “Scanning Near-Field Optical Nanotomography: a New Method of Multiparametric 3D Investigation of Nanostructural Materials”


