Acesso aberto Acesso aberto  Acesso é fechado Acesso está concedido  Acesso é fechado Somente assinantes

Volume 59, Nº 5-6 (2017)

Structure

Microstructure and Substructure of Pearlite in Hypoeutectoid Ferritic-Pearlitic Steels

Kantor M., Vorkachev K.

Resumo

The substructure and microstructure of pearlite in hypoeutectoid low-carbon steel 09G2S is studied using high-contrast images in a scanning electron microscope and electron backscattered diffraction. Acorrelation is established between local deviations from “ideality” in the structure of pearlite and the substructure of pearlitic ferrite. Fragments of pearlitic ferrite, whose development is connected with propagation of long-range misorientations, are seen. It is shown on the basis of visualization that the single-crystal matrix of the pearlitic ferrite consists of individual fragments. These fragments are not generally flat.

Metal Science and Heat Treatment. 2017;59(5-6):265-271
pages 265-271 views

Article

Analysis of Submicrocrystalline Structure Formation Conditions in Iron-Nickel Alloys with Helical Extrusion

Pavlenko D., Tkach D., Kotsyuba V., Beigel’zimer Y.

Resumo

Conditions are analyzed for implementation of helical extrusion of iron-nickel alloy billets with the aim of forming a submicrocrystalline structure within them. Properties are provided for heat-resistant iron-nickel alloys ÉP718-ID (KhN45MVTYuBR ID) and Inconel 718. Two alternative versions are considered for deformation of this type at high and low temperatures. A regime is suggested for helical extrusion of small billets.

Metal Science and Heat Treatment. 2017;59(5-6):272-277
pages 272-277 views

Identification of the “Overburning” Phenomenon for Alloy 2014 Semiproducts

Reznik P., Chikova O., Ovyasnnikov B., Doroshenko N.

Resumo

The microstructure of hardened bars from aluminum alloy 2014 of the Al – Cu – Mg – Si system is analyzed. Metallographic investigation of the morphological features and of the element composition of the structural components of the alloy with features of overburning is performed using scanning electron microscopy and energy dispersion x-ray spectroscopy. The specific symptoms of the phenomenon of “overburning” in alloy 2014 are studied: 1) coarsening of inclusions of a complex chemical composition Al15 (Fe, Mn)3Si2; 2) appearance of intergranular globules about 10 μm in size that form the matrix structure of a copper-rich phase with finely dispersed inclusions of Al15(Fe, Mn)3Si2 phase. The mechanism of structure formation pointing to overburning is considered.

Metal Science and Heat Treatment. 2017;59(5-6):285-288
pages 285-288 views

Increase in Ductility of High Carbon Steel Due to Accelerated Precipitation of Cementite

Ali M., UlHaq E., Ibrahim A., Abdul Karim M., Ali A., Fayyaz M., Khera F.

Resumo

Eutectoid steel AISI 1080 is studied after annealing at 850°C and thermal cycling treatment (TCT) that involves heating at a rate of 10 K/min to 775°C, holding for 10 min, and cooling at a rate of 95 K/min. An increase is established in the content of cementite precipitating over austenite grain boundaries, and relative elongation with retention of yield and ultimate strengths with an increase in number of TCT cycles. After five cycles relative elongation reaches 29% with ultimate strength of 670 MPa.

Metal Science and Heat Treatment. 2017;59(5-6):294-296
pages 294-296 views

Effect of Heat Treatment on the Hardness and Wear of Grinding Balls

Aissat S., Sadeddine A., Bradai M., Younes R., Bilek A., Benabbas A.

Resumo

The effect quenching and tempering by different regimes on Rockwell hardness and wear processes of grinding balls 50 and 70 mm in diameter made of two melts of chromium-molybdenum cast iron is studied. The heating temperature for quenching is 850, 950, and 1050°C; the tempering temperature is 250, 400, and 600°C. Iron is analyzed in an electron microscope. Diffraction patterns are obtained. A model of cast iron wear is suggested and compared to the Davis model and to experimental results. An optimum heat treatment regime is proposed.

Metal Science and Heat Treatment. 2017;59(5-6):297-301
pages 297-301 views

Micro-Arc Diffusion Impregnation of Steel with Carbon and Carbide-Forming Elements

Stepanov M., Dombrovskii Y., Pustovoit V.

Resumo

The possibility of using micro-arc chemical heat treatment in bituminous coal powder for simultaneous impregnation of a steel surface with carbon and carbide-forming elements, i.e., chromium and molybdenum, is studied. Chemical and phase compositions of the diffusion layers are determined. Formation of carbide coatings based on these elements is confirmed.

Metal Science and Heat Treatment. 2017;59(5-6):308-312
pages 308-312 views

Operational Determination of Physical and Mechanical Properties of Cast Samples of High-Strength Iron by Means of a Magnetic-Mechanical Method

Slyusarev Y., Braga A., Slyusarev I.

Resumo

The effect of the chemical composition of high-strength cast iron VCh35 on the content, shape and diameter of graphite inclusions and on the presence of structurally-free cementite and defects is studied. A relationship is determined between the structure and metallurgical defects and characteristics of the mechanical and magnetic rigidity of cast samples. Relationships are established in a group of factors and property characteristics: chemical composition – microstructure – mechanical rigidity – magnetic stiffness. The basis of a method is established making it possible to perform operative non-destructive monitoring of the melt quality preparation for high-strength iron casting.

Metal Science and Heat Treatment. 2017;59(5-6):334-340
pages 334-340 views

Evaluation of Microstructure and Mechanical Properties of High-Strength Bainitic Cast Iron Using an Electromagnetic Sensor

Kashefi M., Nateq M., Kahrobaee S.

Resumo

High-strength bainitic cast iron is studied after isothermal hardening at 340°C for from 0.5 to 5 h with the use of a non-destructive eddy-current method for monitoring the microstructure and mechanical properties. Iron microstructure is studied by optical microscopy and x-ray diffraction analysis. Brinell hardness and the impact energy are determined. Correlation is established between electromagnetic sensor signal, microstructure, and mechanical properties. It is shown that induced voltage and normalized impedance may be used for non-destructive monitoring of the production process and cast iron quality.

Metal Science and Heat Treatment. 2017;59(5-6):341-345
pages 341-345 views

Preparation of A356 Foam Aluminum by Means of Titanium Hydride

Sarajan Z.

Resumo

The effect of heating temperature and stirring time during preparation of foam aluminum alloy A356 on its relative porosity is studied. The optimum amount of the foam-forming agent, i.e., titanium hydride TiH2, facilitating uniform distribution of pores throughout the whole cross section of a hardened casting is determined. Optimum conditions are established for foam formation in a melt during stirring using a mixer are described.

Metal Science and Heat Treatment. 2017;59(5-6):352-356
pages 352-356 views

Effect of Treatment Parameters on Grain Structure and Mechanical Properties of Sheets of Al – 3% Mg Alloy with Zr and Ti Additions

Mochugovskii A., Mikhailovskaya A., Levchenko V., Portnoi V.

Resumo

The microstructure, mechanical properties and superplasticity indices of sheets of aluminum alloy Al – 3% Mg with 0.3% Zr and 0.1% Ti are studied. Use of low-temperature homogenizing (at 360°C) and two-stage hot rolling (at 360 and 420°C) with intermediate annealing at 420°C (3 h) provides quite good thermal stability of alloy grain structure and improved strength properties at room temperature. The alloy exhibits signs of superplasticity with a constant deformation rate of 5 × 10–3 sec–1 and retains a virtually unrecrystallized structure after 200% deformation.

Metal Science and Heat Treatment. 2017;59(5-6):357-362
pages 357-362 views

Effect of Preliminary Quenching on the Efficiency of Hardening Heat Treatment of Cold-Deformed β-Titanium Alloy TS6

Shaboldo O., Mazurov S., Skotnikova M., Shamshurin A., Kononov A.

Resumo

Methods of mechanical testing, metallographic analysis, x-ray diffraction, and back-scattered electron diffraction analysis are used to study β-titanium alloy TS6 wire cold deformed with ε = 45%. It is shown that after ageing alloy with a polygonized structure (quenched from 700°C) has better strength properties than with partial recrystallization (quenching from 800°C).

Metal Science and Heat Treatment. 2017;59(5-6):370-376
pages 370-376 views

Use of Industrial Monitoring Results for Predicting Mechanical Properties of Titanium Alloy Semiproducts

Egorova Y., Uvarov V., Davydenko L., Davydenko R.

Resumo

Ingot chemical composition and the mechanical properties of semiproducts produced at various Russian enterprises from 1971 to 2011 are analyzed. The fundamental possibility is demonstrated for predicting probable values of mechanical properties of wrought titanium alloy semiproducts using industrial monitoring data with errors determined by the contemporary level of industrial production.

Metal Science and Heat Treatment. 2017;59(5-6):377-383
pages 377-383 views

Dynamic Crack Resistance and Steel 09G2S Tubular Billet Structure After Deformation and Heat Treatment

Simonov M., Shaimanov G., Pertsev A., Yurchenko A., Simonov Y.

Resumo

The structure and the dynamic crack resistance of steel 09G2S tubular billets are compared after a heat treatment and different versions of deformation and heat treatment, including cold plastic deformation by radial forging and subsequent annealing. Radial forging followed by annealing has a favorable effect on strength and dynamic crack resistance, which confirms the possibility of industrial use of tubular billets from steel 09G2S after cold radial forging.

Metal Science and Heat Treatment. 2017;59(5-6):389-396
pages 389-396 views

Aluminum Alloys

Alloying Aluminum Alloys with Scandium

Zakharov V., Fisenko I.

Resumo

Methods and procedures are discussed for more economic and effective use of scandium for alloying aluminum alloys. Specifically, it is recommended to introduce scandium and zirconium into aluminum alloys in a 1 : 1 ratio instead of the usual 3 : 1 with the same overall element content. It is also suggested that microalloying with scandium in an amount of 0.1% instead of 0.22% provides the required level of properties in many cases. The possibility of refining the structure of the Al – 2% Sc master alloy for increasing its adaptability (assimilation by the aluminum melt) due to an increase in crystallization rate during ingot casting and other procedures is considered.

Metal Science and Heat Treatment. 2017;59(5-6):278-284
pages 278-284 views

Effect of Iron and Magnesium on Alloy AL9M Structure and Properties

Bazhenov V., Koltygin A., Belov V.

Resumo

The effect of iron impurity on the structure and properties of aluminum alloy AL9M, especially its action on magnesium distribution within the structure, is studied. The microstructure of a cast component of this alloy broken during operation is analyzed. It is shown that iron impurity has an unfavorable effect on structure and mechanical properties of a casting due to appearance of Al9Fe2Si and Al18Fe2Mg7Si10 intermetallics. Formation of these intermetallics consumes a considerable amount of magnesium and lowers the content of the Q(Al5Cu2Mg8Si6) strengthening phase in the alloy structure.

Metal Science and Heat Treatment. 2017;59(5-6):346-351
pages 346-351 views

Heat Treatment

Effect of Isothermal Bainitic Quenching on Rail Steel Impact Strength and Wear Resistance

Çakir F., Çelik O.

Resumo

The effect of heat treatment regimes on hardness, impact strength, and wear resistance of rail steel for high-speed tracks (rail quality category R350HT) is studied. Analysis of steel properties with a different structure is compared: pearlitic, and upper and lower bainite. It is shown that the steel with bainitic structure has the best impact strength, but wear resistance is better for steel with a lower bainite structure.

Metal Science and Heat Treatment. 2017;59(5-6):289-293
pages 289-293 views

Ultra-Jet Diagnosis of Heat Treated Material Microstructure

Bochkarev S., Tsaplin A., Galinovskii A., Abashin M., Barzov A.

Resumo

An ultra-jet diagnosis method for studying the effect of heat treatment regimes on material structure is suggested. Results of experimental studies of hardness, depth of hydraulic cavities, and microstructure of alloy steel specimens after various heat treatment regimes are provided.

Metal Science and Heat Treatment. 2017;59(5-6):384-388
pages 384-388 views

Surface Engineering

Features of Wear-Resistant Cast Iron Coating Formation During Plasma-Powder Surfacing

Vdovin K., Emelyushin A., Nefed’ev S.

Resumo

The structure of coatings deposited on steel 45 by plasma-powder surfacing of white wear-resistant cast iron is studied. The effects of surfacing regime and additional production effects on the welding bath during surfacing produced by current modulation, accelerated cooling of the deposited beads by blowing with air, and accelerated cooling of the substrate with running water on the structure, are determined. A new composition is suggested for powder material for depositing wear-resistant and corrosion-resistant coatings on a carbon steel by the plasma-powder process.

Metal Science and Heat Treatment. 2017;59(5-6):302-307
pages 302-307 views

Friction and Wear

Contact Wear of Steels Kh12M and R6M5

Stepankin I.

Resumo

Comparative analysis of results of contact wear of steels Kh12M and R6M5 is performed with allowance for the structural evolution detected in experimental studies and by computer modeling. It is shown that metal matrix properties determine steel resistance to contact wear and the structural changes arising during wear.

Metal Science and Heat Treatment. 2017;59(5-6):313-320
pages 313-320 views

Technical Information

Study of the Structure and Hardness of Alloys of the Sn – Cu – Co System Used as Diamond Abrasive Tool Binders

Sokolov E., Artem’ev V., Voronova M.

Resumo

The effect of the chemical composition of alloys of the Sn – Cu – Co system used as a binder for diamond abrasive tools on their structure and hardness is studied. It is shown that in the range of concentrations of the elements studied alloy structure is represented by three phases, i.e., β-Co, a solid solution of tin and cobalt in copper (Cu), and an ε (Cu3Sn) intermetallic phase. The lowest microhardness of the three phases is exhibited by β-Co, as a result of which with an increase in cobalt content alloy macrohardness decreases.

Metal Science and Heat Treatment. 2017;59(5-6):321-324
pages 321-324 views

Cast Irons

A Study of the Properties and Structure of Rolling-Mill Iron Modified with Boron

Vdovin K., Zaitseva A., Feoktistov N.

Resumo

The effect of boron additions on the properties and structure of rolling mill iron is studied. The composition of boride phase and carbides, and also the ratio of structural components in iron with different boron contents are determined. Structural transformations in iron during heat treatment are studied by differential thermal analysis and differential scanning calorimetry. The optimum concentration of boron in iron for improving its properties is determined.

Metal Science and Heat Treatment. 2017;59(5-6):327-333
pages 327-333 views

Titanium Alloys

Effect of the Chemical Composition and Structure on the Thermomechanical Behavior of Alloys Based on Titanium Nickelide

Kollerov M., Gusev D., Burnaev A., Sharonov A.

Resumo

The effect of microstructure on the special features of the occurrence of shape change in alloy based on titanium nickelide displaying shape memory and superelasticity is studied. It is shown that total realization of these effects depends not only on alloy structure but also on deformation temperature. Temperature dependences are established for critical strains and stresses governing conditions for total initial shape recovery.

Metal Science and Heat Treatment. 2017;59(5-6):363-369
pages 363-369 views