Vol 22, No 2 (2020)

TECHNOLOGY

Study of the Influence of Technological Parameters on the Strength of a Threaded Connection in Carbon Fiber Parts

Markov A.M., Nekrasov V.N., Salman A.M., Gayst S.V., Su J.

Abstract

Introduction. Composite materials are widely used in mechanical engineering and instrument making. Composites have a low specific gravity with high strength and wear resistance and are used in civil and military equipment. At the same time, the existing technologies for producing composites do not provide sufficient indicators of the parts accuracy; therefore, machining is still the main way to achieve the required quality. Despite the wide technological capabilities of blade processing, high abrasive properties and heterogeneity of the carbon fiber structure imposes a number of limitations and complicates the choice of processing parameters, especially in the manufacture of internal threads. In addition to the processing modes, the diameter of the pre-drilled hole has a significant effect on the quality of the threaded connection. Despite the studies already carried out in the field of machining of carbon fiber reinforced plastics, a number of questions have not received sufficient study. The purpose of the work is to obtain a relationship between the parameters of the hole and thread processing, as well as the diameter of the hole and the quality of the threaded connection to ensure the specified strength characteristics of the threaded connection. A method is proposed and the results of an experimental study of the strength of a threaded joint, consisting of a carbon fiber part with an internal thread and a structural steel screw, are provided in the axial direction with uniform indentation of the screw with the determination of the maximum fracture resistance force. Research methods: a full factorial experiment is conducted for threaded joints with diameters M6, M7 and M8 to identify the dependence of the strength of the threaded connection on such operating parameters as cutting speed and feed rate during drilling and cutting speed when threading. To control the maximum force of fracture resistance, characterizing the strength of the threaded connection, a universal electromechanical testing machine model Instron-3369 is used. Results and discussion. A comparative analysis of the test results shows that for samples with thread diameter M6, the maximum fracture resistance force is from 5.7 to 6.4 kN. But with a minimum supply of drilling in combination with a minimum speed of threading, the maximum load force does not exceed 3.8 kN. Similar results are obtained when testing samples with thread diameters M8 and M10.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):6-15
pages 6-15 views

The Effect of Ultrasonic Impact-Friction Treatment on a Surface Roughness of 09Mn2Si Structural Steel

Lezhnin N.V., Makarov A.V., Luchko S.N., Loginov B.A., Loginov A.B.

Abstract

Introduction. Ultrasonic impact-frictional treatment (UIFT) is a new method of surface strain hardening that improves the properties and refines the microstructure of the surface layer of metallic material. Unlike traditional ultrasonic impact treatment (UIT), the UIFT applies impacts with ultrasonic frequency at an acute angle α to the metal surface in order to activate the shear deformation mode. Oxygen-free atmosphere of argon enhances friction and prevents embrittlement of the diffusion-active deformed layer. A decrease of the angle α during the UIFT leads to a shift of the metal displaced by the tool towards the impact. Therefore, the tool position, oscillating with an ultrasonic frequency, with respect to the tool trajectory may have a profound effect on the surface microrelief. Objective is studying the influence of the impact direction on the roughness and hardening degree of the 09Mn2Si structural steel surface regarding the tool cross-feed during UIFT at an angle α = 50º in the argon medium. Research Methods are following: microhardness measurements, atomic force microscopy (AFM), optical profilometry, optical microscopy and scanning electron microscopy with EBSD analysis. Results and discussion. After grinding, the steel surface microhardness is 200 HV0.1 and the arithmetic mean deviation of the surface profile is Ra= 0.6 μm. UIT at an angle α = 90º in an industrial oil medium results in the surface hardening up to 260 HV0.1, while the Ra parameter increases to 1.6 μm. UIFT with the impact vertical deviation towards the specimen cross-feed (forehand) provides a relatively uniform microrelief with Ra= 0.4 μm and the deformed layer microhardness of up to 500 HV0.1. The tool deviation in the contrary direction towards the specimen cross-feed (backhand) increases the surface hardening degree (620 HV0.1), but leads to the formation of an advanced microrelief consisting of shifted metal displaced by the tool, as well as to the Ra parameter increase up to 3.5 μm. At the same time, the submicrorelief roughness remains approximately at the same level (Ra= 0.03–0.04 μm) for all three hardening treatment methods. Thus, the angle and impact direction during ultrasonic hardening treatment are important technological parameters that allow long-range controlling of the surface microrelief with the UIFT applied as a finishing hardening treatment. UIFT is an effective method of surface hardening, intended to form a surface even with a lower roughness of the microprofile compared to that of a traditional grease-applied UIT.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):16-29
pages 16-29 views

EQUIPMENT. INSTRUMENTS

Morphology and Chemical Composition of the Titanium Alloy Surface at the Initial Stage of Grinding with a Cubic Boron Nitride Wheel

Nosenko V.A., Fetisov A.V., Kuznetsov S.P.

Abstract

Introduction. Intensive adhesive interaction is considered to be one of the main reasons for poor machining of titanium alloys by grinding and mutual transfer of materials in contact. Wear products of the grinding wheel embedded in the treated surface are stress concentrators, which significantly reduces the fatigue strength of the material when operating products under alternating loads. This research area is actively developing and is based on the latest world achievements in the field of surface quality control. To a greater extent, the mutual transfer of materials is considered when grinding wheels made of silicon carbide, to a lesser extent – with wheels made of superhard materials. Objective. Investigation of the morphology and chemical composition of the surface of a titanium alloy after grinding with a wheel of cubic boron nitride on a ceramic bond using the latest world achievements in the field of surface quality control. Methods. The state of the relief and chemical composition of the treated surfaces of the titanium alloy VT1-00 are studied using a FEI Versa 3D LoVac raster two-beam electron microscope immediately after the grinding wheel was corrected and after the specified allowance was removed. Grinding is performed on a precision profile grinding machine CHEVALIER mod. Smart-B1224III. Results and discussion. The condition of the treated surface, obtained immediately after the grinding wheel is corrected, indicates a fairly intensive interaction of the tool with the metal being processed. As the processing time increases, the surface condition improves. Based on morphological studies, wear products of the abrasive tool are found on the surface. Its sizes and distinctive characteristics are determined. By the method of microprobe analysis the chemical composition is established fragments of crystals. According to the atomic content of chemical elements, objects are divided into three groups. Conclusions. The presence of wear products of CBN abrasive tools on a ceramic bundle on the surface of a titanium alloy is experimentally proved: CBN crystals, filler (corundum) and a ceramic bundle. Wear products are embedded in the treated surface.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):30-40
pages 30-40 views

MATERIAL SCIENCE

Assessment of the Heat Parameters Influence on the Process of Electron-Beam Printing of Titanium Alloy Ti64

Kalashnikov K.N., Gurianov D.A., Zykova A.P., Fortuna S.V.

Abstract

Introduction. At present, mainly conventional manufacturing methods, including isothermal forging/forming of hemispheres from titanium alloy workpieces with subsequent welding, are used to create essential components made of titanium alloys, such as high-pressure balloons for rocket engines. These methods are mainly complex multi-stage processes, and therefore the production of titanium balloons can take a very long time and entail high material costs. The technology of wire-feed electron-beam additive manufacturing considered in this work has become proven in the worldwide scientific and industrial community as a technology that allows increasing the productivity of the manufacturing process of various metal components, as well as reducing material costs by minimizing mechanical treatments. However, despite a large number of advantages of this method, technological features of the process, including geometrical parameters of the printed part, such as shape and height of the structure, the angle of the wall inclination from the printing plane, and others, have a significant impact on the formed structure. This is due to the fact that the heat process parameters for different configurations of the printed product will have a different impact on the formation of the structure. In this regard, the purpose of the work is to analyze the influence of heat parameters on the process of printing products from titanium alloy Ti64 using the electron-beam additive manufacturing method to identify regularities of structure formation and material properties at different process parameters. Results and discussion. The conducted researches have shown, that at various combinations of electron-beam 3D-printing process parameters, there is an insignificant change of macrostructure of the obtained Ti64 samples. However, due to different heat inputs and solidification rates, there are differences in microstructure and, therefore, in mechanical properties. The values of ultimate tensile strength and yield strength for obtained samples vary from 851 MPa and 796 MPa to 676 MPa and 574 MPa, respectively.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):41-52
pages 41-52 views

A Review of Experimental Studies of Creep Behavior and Superplasticity in a Discontinuous SiC Aluminum-Matrix Composites

Kryuchkov D.I., Nesterenko A.V.

Abstract

Introduction. Current trends in the development of composite materials based on aluminum alloys discretely hardened by SiC are aimed at structural applications, including at high temperatures. The manufacture of parts using metal forming processes allows to minimize the finishing of workpieces, in which there is a rapid wear of the cutting tool. However, it is necessary to increase the ductility of aluminium matrix composite materials by preliminary deformation-heat treatment. After such treatment, under certain thermomechanical conditions, the composites may exhibit signs of superplasticity. It is also important to be able to predict how external influences (high temperature and pressure) will affect the deformation behavior of composites during operation. Therefore, an integral part of the assessment of the deformation properties of composite materials intended for continuous service is creep testing. At the same time, a joint review of the results of uniaxial tensile tests under creep and superplasticity conditions broadens the picture of the deformation behavior of composite materials in a wide range of temperature-velocity effects. Objective: to conduct a comparative analysis of the results of published studies on the deformation behavior of aluminium matrix composite materials discretely reinforced with silicon carbide during the manifestation of superplasticity and under conditions of high temperature creep. The paper presents the results of published studies of composite materials with matrices based on the following grades of aluminum alloys: Al2009, Al2014, Al2024, Al2124, Al6013, Al6061, Al6063, Al6090, Al8009, Al8090, IN9021. The deformation of aluminium matrix composite materials in the state of superplasticity and under conditions of high temperature creep is considered. Results and discussion. A literature review shows that superplastic deformation mainly manifests itself at strain rates of more than 10–2 s–1. Moreover, the maximum elongation reaches the limits of 200 to 450%. The highest elongation of 685% is obtained at a rate of 5 • 10-4 s-1 for Al2024 / 10SiCp material. In a number of works, it is found that in order to achieve superplastic deformation, the process temperature should be equal to or slightly higher than the temperature of partial melting of the matrix at the grain boundaries of the matrix and the boundaries of the matrix with reinforcing particles. Composite materials with matrices based on the following alloying systems are best studied: Al-Mg-Cu (Al2124), Al-Mg-Si (Al6061), Al-Fe-V-Si (Al8009). Among the factors that most significantly affect the deformation behavior of aluminium matrix composites during creep, it can be noted: the technology of primary production of a composite material, preliminary deformation-heat treatment, the chemical composition of the matrix alloy, and the type and size of the hardening phase. Studies are noted to study the effect of temperature fluctuations on deformation behavior during operation under unsteady creep conditions with a change in pressure. The data collected show that, under certain thermal cycling conditions and low applied pressures, composite materials tend to have high degrees of deformation, which can be promising for developing manufacturing techniques for workpieces and products.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):130-157
pages 130-157 views

Microstructural Features of Welded Railway Frogs formed by Flash Butt Welding and Pulse-Arc Cladding.

Nikulina A.A., Porechina A.A., Khlebnikov S.V., Bataeva Z.B., Potapov V.M.

Abstract

Introduction. Railway crosses (frogs) are important elements of the railway track. In the transition from detachable joints of crosses and rails to permanent connection using butt flash welding, the main problem is to obtain joints characterized by high fracture toughness. The work purpose is to increase the mechanical properties of railway frogs made by welding workpieces from Hadfield steel and rail steel through intermediate alloyed inserts forming by cladding. Materials and methods. Combined constructions between workpieces made from high-carbon and high-manganese steels through an intermediate chromium-nickel insert are analyzed in the work. In the first case, inserts were connected to the workpieces from high-carbon steel by flash butt welding. In the other case, inserts were formed by pulse-arc cladding of A7-IG wire on rail billets. Structural studies are carried out using light microscope and scanning electron microscope equipped with EDX. Microhardness measurements are made with Wolpert Group 402 MVD tester. To determine the strength characteristics, the resulting combined structures are tested according to the three-point bending scheme with the determination of the fracture load and the deflection. Results. It is established that in the joints obtained by pulse-arc cladding of A7-IG wire on rail steel a continuous martensitic layer, which is the main reason for the embrittlement of the joints made by flash butt welding does not appear. The austenite-martensite structure is formed as intermittent layers along the boundaries of dissimilar materials. The maximum microhardness level corresponding to martensitic zones is 680 HV. Three-point bending testing showed that structures in which the intermediate austenitic insert is formed by pulsed-arc cladding, the breaking load and the maximal deflection increased by about 15% comparing with joints fully made by welding.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):53-62
pages 53-62 views

Influence of Electron Beam Additive Manufacturing Process Parameters on Structure and Properties of Austenitic Stainless Steel 321

Zykova A.P., Nikonov S.Y., Utyaganova V.R., Kolubaev E.A.

Abstract

Introduction. In modern industrial and scientific-technical sphere the problem of details formation from various metals and alloys by additive methods is one of the most critical and demanding timely decision. This is primarily due to the need to produce large, complex shaped parts with high productivity and as little waste as possible. One of the most applicable methods for the formation of products by additive method is electron beam wire-feed technology. With use of wire filament and an electron beam for melting in a printing zone it is possible to obtain details with high productivity and acceptable indicators of final structure and mechanical properties. However, interrelation of received structure and mechanical properties depending on parameters of electron beam additive manufacturing process nowadays insufficiently presented in the literature.  In this regard, the purpose of this work is to analyze the influence of additive electron-beam production process parameters on the formation of products from SS 321. Results and discussion. Electron beam current, linear printing speed, and wire feeding ratio are used as variable parameters, and the ultimate tensile strength is taken as the optimization parameter. Optimal parameters of the electron beam current (40 mA), printing speed (180 mm/min) and wire feeding ratio (1.3) at constant accelerating voltage (30 kV) are established. These parameters allow forming the product without defects and without melting the previously formed layers with the ultimate tensile strength of 583 MPa. It is shown that the use of the highest values of printing speed (320 mm/min) and wire feeding ratio (1.3) at varying the electron beam current does not allow to perform the sample formation process. It is established that at the parameters of the electron beam additive manufacturing process, which provide the complete formation of the product, the structures obtained in materials achieve ultimate tensile strength within 558-595 MPa.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):63-75
pages 63-75 views

Study of the Phase Composition and its Effect on the Mechanical Properties of WC- (Fe-Mn-C) Сarbidesteels

Sevostyanova I.N., Sablina T.Y., Fedorov D.V., Golub A.V., Kulkov S.N.

Abstract

Introduction. For development of new composite materials with high static and dynamic strength a great attention is paid to the binder phase. The usage of steels with structural instability, for example, Fe-Mn-C steels as a binder phase of composites, is a promising direction, due to its high ability to strain hardening and the presence of several martensitic transformations. These materials can provide an effective relaxation of stress concentrators arising near carbide particles in the composite during loading of the material due to free form change in the intercarbide space and transfer the external load to the carbide grains. A number of studies are devoted to such research; however, upon preparation of WC- (Fe-Mn-C) carbidesteels, the elemental composition of the binder phase may change due to the technological features of its manufacture by powder metallurgy methods. Therefore, studying the influence of the manganese content changes in the Fe-Mn-C steel binder on the phase composition and mechanical properties of WC-(Fe-Mn-C) materials is very important. The aim of this work is to study the phase composition and its influence on the mechanical properties of WC-(Fe-Mn-C) carbidesteels with changes of the manganese concentration in the matrix. In this work, WC- (Fe-Mn-C) steels are studied, the manganese content in the binder phase is varied from 4 to 18 wt. % . Materials and methods. Carbidesteels are obtained by impregnation of WC carcass with subsequent quenching in oil from 1150 oC. Studies of carbidesteels in initial state and after axial compression test are carried out using X-ray phase and X-ray diffraction analysis, scanning electron microscopy. Results and discussion. The carbide phase content in the obtained carbidesteels is 82 vol. %, the average grain size of tungsten carbide is 2.4 μm, while the porosity does not exceed 0.5%. An increase in the manganese content in the binder phase of carbidesteels leads to a change in the phase composition of the binder phase and to an increase in the lattice parameter of austenite. When the binder phase is in a single-phase state, with a manganese content of 8 wt.%, the maximum relative deformation to failure equal to 6.5% is observed. With an increase in the manganese content in the binder phase, the axial compression strength decreases from 4050 to 3500 MPa. Designed carbidesteels can be used as a different kind of tool. The data obtained can be applied in the development of new composite materials with high physical and mechanical properties.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):76-88
pages 76-88 views

Structure Features and Wear Resistance of Layers, formed by Ni-based Self-fluxing Alloy combined with Boron by Electron Beam, revealed in the Air Atmosphere

Zimogliadova T.A., Bushueva E.G., Shtertser A.A., Grinberg B.E., Soboleva N.N., Kollmannsberger E., Chakin I.K., Bibko D.S., Leonov A.V., Safarova D.E.

Abstract

Introduction. The formation of protective layers on working surfaces of machine parts comprised of chromium-nickel austenitic steels is an effective way to increase its reliability and durability. Ni-base self-fluxing alloys are widely used in order to create wear resistant coatings. The possibility of increasing the set of properties of Ni-Cr-Si-B alloys by adding reinforcing compounds to its matrix or by synthesizing reinforcing phases directly in the process of forming a protective layer is a significant interest of domestic and foreign scientists. The literature does not provide the information on the formation of protective layers on the surface of austenitic steels using cladding by relativistic electron beams of a Ni-Cr-Si-B alloy in combination with hardening additives. Aim of the current work is to increase the tribotechnical properties of the surface layers of steel workpieces via air-revealed electron beam cladding of a Ni-Cr-Si-B alloy in combination with amorphous boron taken in different weight ratios. The proportion of amorphous boron in the powder mixture is 5, 10, and 15 wt. % respectively. The structural features of the cladded layers are investigated by using the following research methods: optical metallography (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and electron microprobe analysis (EMPA). The properties of the surface hardened materials are determined by microhardness investigations and wear resistance during friction against fixed abrasive particles and under conditions of hydroabrasive treatment. Results and discussion. The material produced during cladding of a Ni-Cr-Si-B alloy in combination with 15 wt. % boron is characterized by the maximum microhardness (1000 HV) and wear resistance under various wear conditions. The main structural factor providing an effective increase in the operational characteristics is the formation Fe2B, (Cr, Fe)B borides. It is shown that during Ni-Cr-Si-B alloy +15 wt. % boron cladding precipitation compounds are characterized by phase heterogeneity. The inner part of the two-phase complex particles is CrB2 around which (Fe, Cr)2B is released.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):89-103
pages 89-103 views

Influence of Thermal Effects on the Micromechanical Properties of the Nickel-Chromium Coating obtained by Gas Powder Laser Cladding

Soboleva N.N., Makarov A.V., Stepchenkov A.K., Malygina I.Y., Korobov Y.S.

Abstract

Introduction. Nickel-chromium coatings can be used in parts that are operated at high temperatures (hot deformation dies, rolls of rolling mills, live rolls, parts of turbines, heat exchangers, etc.). A promising method of coating deposition is gas powder laser cladding, which forms coatings with increased hardness and uniformity. A modern method for evaluating the mechanical properties of nickel-chromium coatings is instrumental microindentation, which records diagrams during loading and unloading of the indenter. The aim of the work is to study the effect of thermal action in the temperature range of 800…1050 °C on the micromechanical properties of the NiCrBSi coating PG-10N-01 obtained by gas powder laser cladding. Methods of research are instrumental microindentation and scanning electron microscopy using energy-dispersive microanalysis. Results and discussion. Thermal action at a temperature of 800 °C only slightly reduces the strength characteristics of the coating, while the dissolution of the strengthening phases in the structure of the coating when heated to 900 °C leads to a significant decrease in the hardness characteristics and parameters that characterize the resistance to elastic-plastic deformation. The formation of a “frame-like” structure with a base of large carboborides Cr2(B,C) and borides Cr2B with increased elastic moduli upon heating to 1050 °C (holding for 1 h, cooling in air) leads to a strong increase in the average contact elastic modulus to ~ 280 GPa (with an average level of elastic modulus of ~ 200 GPa in the coating after cladding and after additional heating to 800 and 900 °C). Also, the strength characteristics of microindentation (Martens hardness and indentation hardness at maximum load) and calculated parameters that indicate the improved ability of the coating with a “frame-like” structure to deform in a “favorable” elastic region, as well as to resist mechanical contact loads even after the beginning of the plastic flow, grow to maximum values.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):104-117
pages 104-117 views

Study of the Structure and Mechanical Properties of Aluminum Bronze Printed by Electron Beam Additive Manufacturing

Khoroshko E.S., Filippov A.V., Tarasov S.Y., Shamarin N.N., Kolubaev E.A., Moskvichev E.N., Lychagin D.V.

Abstract

Introduction. The development of additive manufacturing technologies expands the possibilities of manufacturing (printing) products using a variety of materials. The printing process is carried out by local high-energy heating of the filament and substrate, due to which a molten bath is formed. Under such conditions, the formation of the structure of the material occurs under conditions of rapid crystallization and repeated cyclic heating. An important problem in printing bulk products from most structural alloys is the formation of a dendritic structure. The shape and size of dendrites, as well as the formation of secondary phases associated with it, can affect the strength and performance of products. The purpose of the work is to study the structure and mechanical properties of aluminum bronze obtained by the method of electron beam additive production. In this work, the features of the formation of the structure of aluminum bronze depending on the area of the sample are studied. Mechanical tests are carried out under static tension and compression of samples cut in longitudinal and cross sections relative to the direction of printing. The methods of investigation are mechanical tests for compression and tension, optical metallography, scanning electron microscopy. Results and discussion. Based on the analysis of metallographic images, four characteristic types of microstructures are formed at different heights from the substrate in the printed material. The first type is small dendritic grains with intermetallic particles. The second is small dendritic grains. The third is large columnar dendritic grains. Fourth are wide dendritic grains with small inclusions of the secondary phase. The formation of these types of microstructures is due, firstly, to the use of a steel substrate, and secondly, to a change in heat removal conditions as the height of the sample increases during printing. Based on the tests, a significant anisotropy of the mechanical properties was revealed, which is due to the directed nature of the growth of columnar dendritic grains, as well as a change in grain size along the height of the printed material. The obtained results expand the fundamental ideas about the processes of structure formation of alloys in the conditions of electron-beam additive production and can be used in developing technologies for printing products made of copper alloys.
Obrabotka Metallov / Metal Working and Material Science. 2020;22(2):118-129
pages 118-129 views

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